Solution structure of a putative protein disulfide isomerase from Bacteroides thetaiotaomicron
MSLGYIVRIG EMAPDFTITL TDGKQVTLSS LRGKVVMLQF TASWCGVCRK EMPFIEKDIW LKHKDNADFA LIGIDRDEPL EKVLAFAKST GVTYPLGLDP GADIFAKYAL RDAGITRNVL IDREGKIVKL TRLYNEEEFA SLVQQINEML KEGHHHHHH
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 92.7 % (1745 of 1882) | 92.6 % (903 of 975) | 93.3 % (693 of 743) | 90.9 % (149 of 164) |
Backbone | 92.7 % (875 of 944) | 92.9 % (302 of 325) | 93.1 % (433 of 465) | 90.9 % (140 of 154) |
Sidechain | 93.1 % (1010 of 1085) | 92.5 % (601 of 650) | 94.1 % (400 of 425) | 90.0 % (9 of 10) |
Aromatic | 89.0 % (137 of 154) | 89.6 % (69 of 77) | 88.0 % (66 of 75) | 100.0 % (2 of 2) |
Methyl | 100.0 % (196 of 196) | 100.0 % (98 of 98) | 100.0 % (98 of 98) |
1. putative protein disulfide isomerase
MSLGYIVRIG EMAPDFTITL TDGKQVTLSS LRGKVVMLQF TASWCGVCRK EMPFIEKDIW LKHKDNADFA LIGIDRDEPL EKVLAFAKST GVTYPLGLDP GADIFAKYAL RDAGITRNVL IDREGKIVKL TRLYNEEEFA SLVQQINEML KEGHHHHHHSolvent system 90% H2O, 10% D2O, Pressure 1 atm, Temperature 303 K, pH 7.4, Details 20mM Na phosphate buffer, 50mM NaCl, pH 7.4, 1mM DTT, 1mM EDTA
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | putative protein disulfide isomerase | [U-13C; U-15N] | 1 mM | |
2 | sodium phosphate | natural abundance | 20 mM | |
3 | sodium chloride | natural abundance | 50 mM | |
4 | DTT | natural abundance | 1 mM | |
5 | EDTA | natural abundance | 1 mM | |
6 | H2O | natural abundance | 90 % | |
7 | D2O | natural abundance | 10 % |
Solvent system 100% D2O, Pressure 1 atm, Temperature 303 K, pH 7.4, Details 20mM Na phosphate buffer, 50mM NaCl, pH 7.4, 1mM DTT, 1mM EDTA
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
8 | putative protein disulfide isomerase | [U-13C; U-15N] | 1 mM | |
9 | sodium phosphate | natural abundance | 20 mM | |
10 | sodium chloride | natural abundance | 50 mM | |
11 | DTT | natural abundance | 1 mM | |
12 | EDTA | natural abundance | 1 mM | |
13 | D2O | natural abundance | 100 % |