High resolution NMR structure of the theta-defensin HTD-2 (retrocyclin 2)
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 82.7 % (163 of 197) | 96.2 % (102 of 106) | 68.5 % (50 of 73) | 61.1 % (11 of 18) |
Backbone | 74.1 % (80 of 108) | 100.0 % (39 of 39) | 58.8 % (30 of 51) | 61.1 % (11 of 18) |
Sidechain | 90.4 % (94 of 104) | 94.0 % (63 of 67) | 83.8 % (31 of 37) | |
Methyl | 100.0 % (16 of 16) | 100.0 % (8 of 8) | 100.0 % (8 of 8) |
1. HTD-2
GICRCICGRR ICRCICGRSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 5.0 (±1.0), Details 1.0 mM, pH 5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | HTD-2 | natural abundance | 1.0 mM | |
2 | H2O | natural abundance | 90 % | |
3 | D2O | natural abundance | 10 % |
Solvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 5.0 (±1.0), Details 1.0 mM, pH 5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
4 | HTD-2 | natural abundance | 1.0 mM | |
5 | D2O | natural abundance | 100 % |