1H, 13C and 15N Chemical Shift Assignments for Phl p 5a
PAGKATTEEQ KLIEKINAGF KAALAAAAGV QPADKYRTFV ATFGAASNKA FAEGLSGEPK GAAESSSKAA LTSKLDAAYK LAYKTAEGAT PEAKYDAYVA TLSEALRIIA GTLEVHAVKP AAEEVKVIPA GELQVIEKVD AAFKVAATAA NAAPANDKFT VFEAAFNDAI KASTGGAYES YKFIPALEAA VKQAYAATVA TAPEVKYTVF ETALKKAITA MSEAQKAAKP A
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 92.7 % (2331 of 2515) | 91.2 % (1167 of 1279) | 94.0 % (945 of 1005) | 94.8 % (219 of 231) |
Backbone | 97.4 % (1331 of 1366) | 97.6 % (453 of 464) | 96.9 % (660 of 681) | 98.6 % (218 of 221) |
Sidechain | 88.8 % (1215 of 1368) | 87.6 % (714 of 815) | 92.1 % (500 of 543) | 10.0 % (1 of 10) |
Aromatic | 83.0 % (146 of 176) | 84.1 % (74 of 88) | 81.8 % (72 of 88) | |
Methyl | 97.7 % (295 of 302) | 98.0 % (148 of 151) | 97.4 % (147 of 151) |
1. entity
PAGKATTEEQ KLIEKINAGF KAALAAAAGV QPADKYRTFV ATFGAASNKA FAEGLSGEPK GAAESSSKAA LTSKLDAAYK LAYKTAEGAT PEAKYDAYVA TLSEALRIIA GTLEVHAVKP AAEEVKVIPA GELQVIEKVD AAFKVAATAA NAAPANDKFT VFEAAFNDAI KASTGGAYES YKFIPALEAA VKQAYAATVA TAPEVKYTVF ETALKKAITA MSEAQKAAKP ASolvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 297 K, pH 6.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Phl | natural abundance | 0.0 mM | |
2 | D2O | natural abundance | 7 % | |
3 | H2O | natural abundance | 93 % |
Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 297 K, pH 6.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
4 | Phl | natural abundance | 0.0 mM | |
5 | D2O | natural abundance | 7 % | |
6 | H2O | natural abundance | 93 % |
Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 297 K, pH 6.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | Phl | natural abundance | 0.0 mM | |
8 | D2O | natural abundance | 7 % | |
9 | H2O | natural abundance | 93 % |