Solution structure of RasGRP2 EF hands bound to calcium
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 76.4 % (720 of 943) | 69.0 % (338 of 490) | 83.3 % (304 of 365) | 88.6 % (78 of 88) |
Backbone | 96.7 % (468 of 484) | 96.4 % (163 of 169) | 97.0 % (228 of 235) | 96.2 % (77 of 80) |
Sidechain | 60.9 % (324 of 532) | 54.5 % (175 of 321) | 72.9 % (148 of 203) | 12.5 % (1 of 8) |
Aromatic | 5.3 % (5 of 94) | 10.6 % (5 of 47) | 0.0 % (0 of 47) | |
Methyl | 89.5 % (68 of 76) | 81.6 % (31 of 38) | 97.4 % (37 of 38) |
1. RasGRP2
KLDQALVVEH IEKMVESVFR NFDVDGDGHI SQEEFQIIRG NFPYLSAFGD LDQNQDGCIS REEMVSYFLR SSSVLGGRMG FSolvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 304 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | RasGRP2 | [U-99% 13C; U-99% 15N] | 500 uM | |
2 | HEPES | natural abundance | 25 mM | |
3 | sodium chloride | natural abundance | 100 mM | |
4 | TCEP | natural abundance | 1 mM | |
5 | D2O | natural abundance | 7 % | |
6 | H2O | natural abundance | 93 % |
Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 304 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | RasGRP2 | [U-99% 13C; U-99% 15N] | 500 uM | |
8 | HEPES | natural abundance | 25 mM | |
9 | sodium chloride | natural abundance | 100 mM | |
10 | TCEP | natural abundance | 1 mM | |
11 | D2O | natural abundance | 7 % | |
12 | H2O | natural abundance | 93 % | |
13 | Pf1 phage | natural abundance | 17 mg/mL |