NMR structure of DNA duplex
Polymer type: polydeoxyribonucleotide
Total | 1H | 31P | |
---|---|---|---|
All | 86.2 % (150 of 174) | 86.1 % (136 of 158) | 87.5 % (14 of 16) |
Suger, PO4 | 98.4 % (126 of 128) | 100.0 % (112 of 112) | 87.5 % (14 of 16) |
Nucleobase | 52.2 % (24 of 46) | 52.2 % (24 of 46) | |
Aromatic | 75.0 % (24 of 32) | 75.0 % (24 of 32) | |
Methyl | 0.0 % (0 of 2) | 0.0 % (0 of 2) |
1. DNA (5'-D(*GP*TP*CP*GP*GP*CP*TP*G)-3')
GTCGGCTG2. DNA (5'-D(*CP*AP*GP*CP*CP*GP*AP*C)-3')
CAGCCGACSolvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | DNA (5'-D(*GP*TP*CP*GP*GP*CP*TP*G)-3') | natural abundance | 0.5 mM | |
2 | DNA (5'-D(*CP*AP*GP*CP*CP*GP*AP*C)-3') | natural abundance | 0.5 mM | |
3 | D2O | [U-100% 2H] | 100 % | |
4 | sodium chloride | natural abundance | 50 mM | |
5 | sodium phosphate | natural abundance | 10 mM | |
6 | EDTA | natural abundance | 0.1 mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | DNA (5'-D(*GP*TP*CP*GP*GP*CP*TP*G)-3') | natural abundance | 0.5 mM | |
8 | DNA (5'-D(*CP*AP*GP*CP*CP*GP*AP*C)-3') | natural abundance | 0.5 mM | |
9 | D2O | [U-100% 2H] | 10 % | |
10 | H2O | natural abundance | 90 % | |
11 | sodium chloride | natural abundance | 50 mM | |
12 | sodium phosphate | natural abundance | 10 mM | |
13 | EDTA | natural abundance | 0.1 mM |
Polymer type: polydeoxyribonucleotide
Total | 1H | 31P | |
---|---|---|---|
All | 48.9 % (170 of 348) | 49.4 % (156 of 316) | 43.8 % (14 of 32) |
Suger, PO4 | 49.2 % (126 of 256) | 50.0 % (112 of 224) | 43.8 % (14 of 32) |
Nucleobase | 47.8 % (44 of 92) | 47.8 % (44 of 92) | |
Aromatic | 46.9 % (30 of 64) | 46.9 % (30 of 64) | |
Methyl | 50.0 % (2 of 4) | 50.0 % (2 of 4) |
1. DNA (5'-D(*GP*TP*CP*GP*GP*CP*TP*G)-3')
GTCGGCTG2. DNA (5'-D(*CP*AP*GP*CP*CP*GP*AP*C)-3')
CAGCCGACSolvent system 100% D2O, Pressure 1 atm, Temperature 283 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | DNA (5'-D(*GP*TP*CP*GP*GP*CP*TP*G)-3') | natural abundance | 0.5 mM | |
2 | DNA (5'-D(*CP*AP*GP*CP*CP*GP*AP*C)-3') | natural abundance | 0.5 mM | |
3 | D2O | [U-100% 2H] | 100 % | |
4 | sodium chloride | natural abundance | 50 mM | |
5 | sodium phosphate | natural abundance | 10 mM | |
6 | EDTA | natural abundance | 0.1 mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 283 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | DNA (5'-D(*GP*TP*CP*GP*GP*CP*TP*G)-3') | natural abundance | 0.5 mM | |
8 | DNA (5'-D(*CP*AP*GP*CP*CP*GP*AP*C)-3') | natural abundance | 0.5 mM | |
9 | D2O | [U-100% 2H] | 10 % | |
10 | H2O | natural abundance | 90 % | |
11 | sodium chloride | natural abundance | 50 mM | |
12 | sodium phosphate | natural abundance | 10 mM | |
13 | EDTA | natural abundance | 0.1 mM |