Backbone 1H, 13C, and 15N Chemical Shift Assignments for murine norovirus CR6 NS1/2 protein
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 61.4 % (493 of 803) | 75.7 % (318 of 420) | 38.7 % (122 of 315) | 77.9 % (53 of 68) |
Backbone | 68.2 % (277 of 406) | 78.4 % (109 of 139) | 57.9 % (117 of 202) | 78.5 % (51 of 65) |
Sidechain | 58.4 % (269 of 461) | 74.4 % (209 of 281) | 32.8 % (58 of 177) | 66.7 % (2 of 3) |
Aromatic | 34.1 % (30 of 88) | 63.6 % (28 of 44) | 0.0 % (0 of 42) | 100.0 % (2 of 2) |
Methyl | 68.3 % (41 of 60) | 100.0 % (30 of 30) | 36.7 % (11 of 30) |
1. entity
MRGSHHHHHH GSGALAALHA DGPHAGLPVT RSDARVLIFN DWEERKRSEP WLRLDMSDKA IFRRYPHLRSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 273 K, pH 7.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | sodium phosphate | natural abundance | 50 mM | |
2 | sodium chloride | natural abundance | 300 mM | |
3 | entity | natural abundance | 0.5 mM | |
4 | DSS | natural abundance | 0 mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 273 K, pH 7.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | sodium phosphate | natural abundance | 50 mM | |
6 | sodium chloride | natural abundance | 300 mM | |
7 | entity | [U-100% 13C; U-100% 15N] | 0.5 mM | |
8 | DSS | natural abundance | 0 mM |