Backbone resonance assignments of the pyrin domain of human Pyrin
MAKTPSDHLL STLEELVPYD FEKFKFKLQN TSVQKEHSRI PRSQIQRARP VKMATLLVTY YGEEYAVQLT LQVLRAINQR LLAEELHRAA IQLEHHHHHH
Polymer type: polypeptide(D)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 52.8 % (650 of 1230) | 37.3 % (240 of 643) | 65.3 % (314 of 481) | 90.6 % (96 of 106) |
Backbone | 98.3 % (582 of 592) | 97.5 % (192 of 197) | 99.3 % (297 of 299) | 96.9 % (93 of 96) |
Sidechain | 22.7 % (167 of 737) | 10.8 % (48 of 446) | 41.3 % (116 of 281) | 30.0 % (3 of 10) |
Aromatic | 10.2 % (10 of 98) | 12.2 % (6 of 49) | 8.2 % (4 of 49) | |
Methyl | 16.9 % (21 of 124) | 11.3 % (7 of 62) | 22.6 % (14 of 62) |
1. Pyrin
MAKTPSDHLL STLEELVPYD FEKFKFKLQN TSVQKEHSRI PRSQIQRARP VKMATLLVTY YGEEYAVQLT LQVLRAINQR LLAEELHRAA IQLEHHHHHHSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 4.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Pyrin | [U-100% 13C; U-100% 15N] | 0.8 mM | |
2 | H2O | natural abundance | 90 % | |
3 | D2O | natural abundance | 10 % |