NMR structure of Copsin
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 90.5 % (517 of 571) | 98.6 % (292 of 296) | 77.0 % (167 of 217) | 100.0 % (58 of 58) |
Backbone | 84.2 % (278 of 330) | 97.4 % (112 of 115) | 70.4 % (114 of 162) | 98.1 % (52 of 53) |
Sidechain | 96.9 % (282 of 291) | 97.8 % (177 of 181) | 95.2 % (100 of 105) | 100.0 % (5 of 5) |
Aromatic | 88.9 % (16 of 18) | 100.0 % (9 of 9) | 77.8 % (7 of 9) | |
Methyl | 91.3 % (42 of 46) | 91.3 % (21 of 23) | 91.3 % (21 of 23) |
1. entity
XNCPTRRGLC VTSGLTACRN HCRSCHRGDV GCVRCSNAQC TGFLGTTCTC INPCPRCSolvent system 100% D2O, Pressure 1 atm, Temperature 293 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | sodium phosphate | natural abundance | 20 mM | |
2 | sodium chloride | natural abundance | 50 mM | |
3 | D2O | natural abundance | 100 % | |
4 | Copsin | [U-13C; U-15N] |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 293 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | sodium phosphate | natural abundance | 20 mM | |
6 | sodium chloride | natural abundance | 50 mM | |
7 | D2O | natural abundance | 10 % | |
8 | Copsin | [U-13C; U-15N] | ||
9 | H2O | natural abundance | 90 % |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 89.8 % (1025 of 1142) | 97.5 % (577 of 592) | 76.7 % (333 of 434) | 99.1 % (115 of 116) |
Backbone | 84.2 % (556 of 660) | 96.5 % (222 of 230) | 71.0 % (230 of 324) | 98.1 % (104 of 106) |
Sidechain | 96.4 % (561 of 582) | 97.2 % (352 of 362) | 94.8 % (199 of 210) | 100.0 % (10 of 10) |
Aromatic | 88.9 % (32 of 36) | 100.0 % (18 of 18) | 77.8 % (14 of 18) | |
Methyl | 91.3 % (84 of 92) | 91.3 % (42 of 46) | 91.3 % (42 of 46) |
1. entity
XNCPTRRGLC VTSGLTACRN HCRSCHRGDV GCVRCSNAQC TGFLGTTCTC INPCPRCSolvent system 100% D2O, Pressure 1 atm, Temperature 293 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | sodium phosphate | natural abundance | 20 mM | |
2 | sodium chloride | natural abundance | 50 mM | |
3 | D2O | natural abundance | 100 % | |
4 | Copsin | [U-13C; U-15N] |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 293 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | sodium phosphate | natural abundance | 20 mM | |
6 | sodium chloride | natural abundance | 50 mM | |
7 | D2O | natural abundance | 10 % | |
8 | Copsin | [U-13C; U-15N] | ||
9 | H2O | natural abundance | 90 % |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 90.0 % (1542 of 1713) | 98.2 % (872 of 888) | 76.3 % (497 of 651) | 99.4 % (173 of 174) |
Backbone | 84.2 % (834 of 990) | 97.4 % (336 of 345) | 70.2 % (341 of 486) | 98.7 % (157 of 159) |
Sidechain | 97.4 % (850 of 873) | 98.2 % (533 of 543) | 95.9 % (302 of 315) | 100.0 % (15 of 15) |
Aromatic | 88.9 % (48 of 54) | 100.0 % (27 of 27) | 77.8 % (21 of 27) | |
Methyl | 94.2 % (130 of 138) | 94.2 % (65 of 69) | 94.2 % (65 of 69) |
1. entity
XNCPTRRGLC VTSGLTACRN HCRSCHRGDV GCVRCSNAQC TGFLGTTCTC INPCPRCSolvent system 100% D2O, Pressure 1 atm, Temperature 293 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | sodium phosphate | natural abundance | 20 mM | |
2 | sodium chloride | natural abundance | 50 mM | |
3 | D2O | natural abundance | 100 % | |
4 | Copsin | [U-13C; U-15N] |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 293 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | sodium phosphate | natural abundance | 20 mM | |
6 | sodium chloride | natural abundance | 50 mM | |
7 | D2O | natural abundance | 10 % | |
8 | Copsin | [U-13C; U-15N] | ||
9 | H2O | natural abundance | 90 % |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 90.3 % (2063 of 2284) | 98.6 % (1167 of 1184) | 76.6 % (665 of 868) | 99.6 % (231 of 232) |
Backbone | 84.5 % (1116 of 1320) | 97.8 % (450 of 460) | 70.4 % (456 of 648) | 99.1 % (210 of 212) |
Sidechain | 97.9 % (1139 of 1164) | 98.6 % (714 of 724) | 96.4 % (405 of 420) | 100.0 % (20 of 20) |
Aromatic | 88.9 % (64 of 72) | 100.0 % (36 of 36) | 77.8 % (28 of 36) | |
Methyl | 95.7 % (176 of 184) | 95.7 % (88 of 92) | 95.7 % (88 of 92) |
1. entity
XNCPTRRGLC VTSGLTACRN HCRSCHRGDV GCVRCSNAQC TGFLGTTCTC INPCPRCSolvent system 100% D2O, Pressure 1 atm, Temperature 293 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | sodium phosphate | natural abundance | 20 mM | |
2 | sodium chloride | natural abundance | 50 mM | |
3 | D2O | natural abundance | 100 % | |
4 | Copsin | [U-13C; U-15N] |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 293 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | sodium phosphate | natural abundance | 20 mM | |
6 | sodium chloride | natural abundance | 50 mM | |
7 | D2O | natural abundance | 10 % | |
8 | Copsin | [U-13C; U-15N] | ||
9 | H2O | natural abundance | 90 % |