1H, 13C, and 15N Chemical Shift Assignments for Thymosin alpha 1
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 85.4 % (258 of 302) | 92.9 % (145 of 156) | 71.8 % (84 of 117) | 100.0 % (29 of 29) |
Backbone | 83.9 % (141 of 168) | 100.0 % (56 of 56) | 67.9 % (57 of 84) | 100.0 % (28 of 28) |
Sidechain | 88.3 % (143 of 162) | 89.0 % (89 of 100) | 86.9 % (53 of 61) | 100.0 % (1 of 1) |
Methyl | 81.3 % (26 of 32) | 81.3 % (13 of 16) | 81.3 % (13 of 16) |
1. Thymosin alpha 1 polypeptide
XSDAAVDTSS EITTKDLKEK KEVVEEAENSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Thymosin alpha 1 polypeptide | natural abundance | 8 mM | |
2 | SDS | [U-100% 2H] | 80 mM | |
3 | H2O | natural abundance | 90 % | |
4 | D2O | natural abundance | 10 % |