BMRB: 21054

Solution structure of the amphibian egg glycan Bv9 from Bombina variegata

Authors

Schubert, M., Allain, F.

Assembly

Bv9(trisaccharide)

Entity

1. Bv9(trisaccharide) (polymer, Thiol state: not present), 4 monomers, 566.5522 Da

Formula weight

566.5522 Da

Source organism

Bombina variegata variegata

Exptl. method

solution NMR

Data set

assigned_chemical_shifts

Chemcal Shifts

¹H: 38, ¹³C: 28 assignments Detail

Download

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ID	Entity ID	Seq ID	Comp ID	Atom ID	Atom type	Val	Val err	Ambig. code
1	1	1	SP	H11	H	3.594	0.005	2
2	1	1	SP	H12	H	3.503	0.005	2
3	1	1	SP	H2	H	4.231	0.005	1
4	1	1	SP	H3	H	5.764	0.005	4
5	1	1	SP	H4	H	5.762	0.009	4
6	1	1	SP	H5	H	4.321	0.009	1
7	1	1	SP	H61	H	3.892	0.005	2
8	1	1	SP	H62	H	3.500	0.005	2
9	1	1	SP	C1	C	67.505	0.050	1
10	1	1	SP	C2	C	74.651	0.050	1
11	1	1	SP	C3	C	133.696	0.050	4
12	1	1	SP	C4	C	133.696	0.050	4
13	1	1	SP	C5	C	73.154	0.050	1
14	1	1	SP	C6	C	75.978	0.050	1
15	1	2	MAG	H1	H	4.443	0.005	1
16	1	2	MAG	H2	H	3.849	0.005	1
17	1	2	MAG	H3	H	3.974	0.005	1
18	1	2	MAG	H4	H	3.728	0.005	1
19	1	2	MAG	H5	H	3.501	0.005	1
20	1	2	MAG	H61	H	3.956	0.005	2
21	1	2	MAG	H62	H	3.865	0.005	2
22	1	2	MAG	H81	H	2.081	0.005	1
23	1	2	MAG	H82	H	2.081	0.005	1
24	1	2	MAG	H83	H	2.081	0.005	1
25	1	2	MAG	HN2	H	8.498	0.005	1
26	1	2	MAG	C1	C	104.535	0.050	1
27	1	2	MAG	C2	C	58.332	0.050	1
28	1	2	MAG	C3	C	78.768	0.050	1
29	1	2	MAG	C4	C	74.956	0.070	1
30	1	2	MAG	C5	C	77.917	0.050	1
31	1	2	MAG	C6	C	62.223	0.050	1
32	1	2	MAG	C7	C	176.835	0.050	1
33	1	2	MAG	C8	C	25.026	0.050	1
34	1	3	NAG	H1	H	4.621	0.005	1
35	1	3	NAG	H2	H	3.629	0.005	1
36	1	3	NAG	H3	H	3.587	0.005	1
37	1	3	NAG	H4	H	3.188	0.005	1
38	1	3	NAG	H5	H	3.386	0.005	1
39	1	3	NAG	H61	H	3.974	0.005	2
40	1	3	NAG	H62	H	3.572	0.005	2
41	1	3	NAG	H81	H	1.990	0.005	1
42	1	3	NAG	H82	H	1.990	0.005	1
43	1	3	NAG	H83	H	1.990	0.005	1
44	1	3	NAG	HN2	H	8.095	0.005	1
45	1	3	NAG	C1	C	103.939	0.050	1
46	1	3	NAG	C2	C	58.685	0.050	1
47	1	3	NAG	C3	C	75.671	0.050	1
48	1	3	NAG	C4	C	73.383	0.050	1
49	1	3	NAG	C5	C	78.485	0.050	1
50	1	3	NAG	C6	C	64.384	0.050	1
51	1	3	NAG	C7	C	177.393	0.050	1
52	1	3	NAG	C8	C	25.020	0.050	1
53	1	4	FUC	H1	H	5.022	0.005	1
54	1	4	FUC	H2	H	3.795	0.005	1
55	1	4	FUC	H3	H	3.916	0.005	1
56	1	4	FUC	H4	H	3.796	0.005	1
57	1	4	FUC	H5	H	4.853	0.005	1
58	1	4	FUC	H61	H	1.274	0.005	1
59	1	4	FUC	H62	H	1.274	0.005	1
60	1	4	FUC	H63	H	1.274	0.005	1
61	1	4	FUC	C1	C	100.791	0.050	1
62	1	4	FUC	C2	C	70.356	0.050	1
63	1	4	FUC	C3	C	71.714	0.050	1
64	1	4	FUC	C4	C	74.705	0.050	1
65	1	4	FUC	C5	C	69.434	0.050	1
66	1	4	FUC	C6	C	18.250	0.050	1

Release date

2014-01-29

Citation

A Secondary Structural Element in a Wide Range of Fucosylated Glycoepitopes
Aeschbacher, T., Zierke, M., Smiesko, M., Collot, M., Mallet, J.M., Ernst, B., Allain, F.H., Schubert, M.
Chemistry (2017), 23, 11598-11610, PubMed 28654715 , DOI 10.1002/chem.201701866 , Abstract

Entries sharing articles BMRB: 4 entries Detail

Experiments performed 5 experiments Detail

Chemical shift validation 3 contents Detail