STRUCTURAL CHARACTERIZATION OF THE C3 DOMAIN OF CARDIAC MYOSIN BINDING PROTEIN-C
GSHMPVLITR PLEDQLVMVG QRVEFECEVS EEGAQVKWLK DGVELTREET FKYRFKKDGQ RHHLIINEAM LEDAGHYALC TSGGQALAEL IVQEK
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 96.8 % (1078 of 1114) | 96.2 % (559 of 581) | 97.7 % (422 of 432) | 96.0 % (97 of 101) |
Backbone | 97.0 % (549 of 566) | 95.9 % (188 of 196) | 98.2 % (272 of 277) | 95.7 % (89 of 93) |
Sidechain | 96.9 % (615 of 635) | 96.4 % (371 of 385) | 97.5 % (236 of 242) | 100.0 % (8 of 8) |
Aromatic | 97.3 % (72 of 74) | 100.0 % (37 of 37) | 94.4 % (34 of 36) | 100.0 % (1 of 1) |
Methyl | 100.0 % (108 of 108) | 100.0 % (54 of 54) | 100.0 % (54 of 54) |
1. entity
GSHMPVLITR PLEDQLVMVG QRVEFECEVS EEGAQVKWLK DGVELTREET FKYRFKKDGQ RHHLIINEAM LEDAGHYALC TSGGQALAEL IVQEKSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | sodium phosphate | natural abundance | 50 mM | |
2 | sodium chloride | natural abundance | 100 mM | |
3 | protein | [U-100% 13C; U-100% 15N] | 0.8 mM | |
4 | H2O | natural abundance | 90 % | |
5 | D2O | natural abundance | 10 % |