NMR structure of the Mycobacterium tuberculosis LppM (Rv2171) protein folded domain.
GRENLYFQGH MLRVRASITI SPDDLVSGEI IAAAKPKNSK DTGPALDGDV PFSQKVAVSN YDSDGYVGSQ AVFSDLTFAE LPQLANMNSD AAGVNLSLRR NGNIVILEGR ADLTSVSDPD ADVELTVAFP AAVTSTNGDR IEPEVVQWKL KPGVVSTMSA QARYTDPNTR S
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 83.4 % (1555 of 1864) | 92.1 % (882 of 958) | 69.1 % (503 of 728) | 95.5 % (170 of 178) |
Backbone | 94.2 % (948 of 1006) | 95.1 % (327 of 344) | 93.4 % (468 of 501) | 95.0 % (153 of 161) |
Sidechain | 74.3 % (756 of 1017) | 90.4 % (555 of 614) | 47.7 % (184 of 386) | 100.0 % (17 of 17) |
Aromatic | 49.0 % (48 of 98) | 83.7 % (41 of 49) | 12.5 % (6 of 48) | 100.0 % (1 of 1) |
Methyl | 64.2 % (131 of 204) | 98.0 % (100 of 102) | 30.4 % (31 of 102) |
1. entity
GRENLYFQGH MLRVRASITI SPDDLVSGEI IAAAKPKNSK DTGPALDGDV PFSQKVAVSN YDSDGYVGSQ AVFSDLTFAE LPQLANMNSD AAGVNLSLRR NGNIVILEGR ADLTSVSDPD ADVELTVAFP AAVTSTNGDR IEPEVVQWKL KPGVVSTMSA QARYTDPNTR SSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 (±1) K, pH 6.8 (±0.034)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | entity | [U-100% 15N] | 0.9 (±0.0045) mM | |
2 | sodium phosphate | natural abundance | 25 (±0.125) mM | |
3 | sodium chloride | natural abundance | 150 (±0.75) mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 (±1) K, pH 6.8 (±0.034)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
4 | entity | [U-100% 13C; U-100% 15N] | 0.9 (±0.0045) mM | |
5 | sodium phosphate | natural abundance | 25 (±0.125) mM | |
6 | sodium chloride | natural abundance | 150 (±0.75) mM |