92% Backbone 1H, 13C, and 15N Chemical Shift Assignments for New Delhi beta lactamase 1 (without Zinc)
MGEIRPTIGQ QMETGDQRFG DLVFRQLAPN VWQHTSYLDM PGFGAVASNG LIVRDGGRVL VVDTAWTDDQ TAQILNWIKQ EINLPVALAV VTHAHQDKMG GMDALHAAGI ATYANALSNQ LAPQEGMVAA QHSLTFAANG WVEPATAPNF GPLKVFYPGP GHTSDNITVG IDGTDIAFGG CLIKDSKAKS LGNLGDADTE HYAASARAFG AAFPKASMIV MSHSAPDSRA AITHTARMAD KLRLEHHHHH HHH
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 38.5 % (1073 of 2785) | 16.1 % (228 of 1417) | 57.2 % (625 of 1092) | 79.7 % (220 of 276) |
Backbone | 71.9 % (1074 of 1494) | 44.0 % (228 of 518) | 85.0 % (625 of 735) | 91.7 % (221 of 241) |
Sidechain | 11.4 % (173 of 1520) | 0.0 % (0 of 899) | 29.5 % (173 of 586) | 0.0 % (0 of 35) |
Aromatic | 0.0 % (0 of 238) | 0.0 % (0 of 119) | 0.0 % (0 of 115) | 0.0 % (0 of 4) |
Methyl | 11.8 % (34 of 288) | 0.0 % (0 of 144) | 23.6 % (34 of 144) |
1. New Delhi Beta Lactamase 1
MGEIRPTIGQ QMETGDQRFG DLVFRQLAPN VWQHTSYLDM PGFGAVASNG LIVRDGGRVL VVDTAWTDDQ TAQILNWIKQ EINLPVALAV VTHAHQDKMG GMDALHAAGI ATYANALSNQ LAPQEGMVAA QHSLTFAANG WVEPATAPNF GPLKVFYPGP GHTSDNITVG IDGTDIAFGG CLIKDSKAKS LGNLGDADTE HYAASARAFG AAFPKASMIV MSHSAPDSRA AITHTARMAD KLRLEHHHHH HHHSolvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 293 K, pH 6.5, Details 50mM phosphate sodium pH 6.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | New Delhi Beta Lactamase 1 | [U-100% 13C; U-100% 15N; U-80% 2H] | 0.75 mM | |
2 | phosphate sodium | natural abundance | 50 mM |