NMR Structure of NS5A-D2 (JFH1) peptide (304-323)
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 81.3 % (195 of 240) | 88.2 % (112 of 127) | 68.8 % (66 of 96) | 100.0 % (17 of 17) |
Backbone | 95.5 % (105 of 110) | 94.4 % (34 of 36) | 94.9 % (56 of 59) | 100.0 % (15 of 15) |
Sidechain | 73.2 % (109 of 149) | 85.7 % (78 of 91) | 51.8 % (29 of 56) | 100.0 % (2 of 2) |
Aromatic | 23.3 % (7 of 30) | 40.0 % (6 of 15) | 0.0 % (0 of 14) | 100.0 % (1 of 1) |
Methyl | 66.7 % (12 of 18) | 100.0 % (9 of 9) | 33.3 % (3 of 9) |
1. entity 1
GFPRALPAWA RPDYNPPLVESolvent system 95% H2O/5% D2O, Pressure 1 bar, Temperature 298 K, pH 6.4, Details 5 mM unlabelled NS5A-D2(JFH1)peptide 304-323, 95% H2O/5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | NS5A-D2(JFH1)peptide 304-323 | unlabelled | 5 mM | |
2 | NaCl | natural abundance | 30 mM |
Solvent system 95% H2O/5% D2O, Pressure 1 bar, Temperature 298 K, pH 6.4, Details 1 mM [U-99% 13C; U-99% 15N] 15N 13C NS5A-D2(JFH1)peptide 304-323, 95% H2O/5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
3 | 15N 13C NS5A-D2(JFH1)peptide 304-323 | [U-99% 13C; U-99% 15N] | 1 mM | |
4 | NaCl | natural abundance | 30 mM |