Ocellatin-LB1, solution structure in DPC micelle by NMR spectroscopy
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 83.8 % (197 of 235) | 89.9 % (107 of 119) | 73.4 % (69 of 94) | 95.5 % (21 of 22) |
Backbone | 82.6 % (109 of 132) | 97.9 % (46 of 47) | 66.7 % (42 of 63) | 95.5 % (21 of 22) |
Sidechain | 87.7 % (107 of 122) | 84.7 % (61 of 72) | 92.0 % (46 of 50) | |
Aromatic | 25.0 % (1 of 4) | 50.0 % (1 of 2) | 0.0 % (0 of 2) | |
Methyl | 100.0 % (36 of 36) | 100.0 % (18 of 18) | 100.0 % (18 of 18) |
1. entity 1
GVVDILKGAA KDIAGHLASK VMXSolvent system trifluoroethanol/water, Pressure 1 atm, Temperature 273.15 K, pH 4, Details 1.5 mM Ocellatin-LB1, 400 mM d38 DPC, 5 % 99.75% D2O, trifluoroethanol/water.
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | D2O | [U-99.75 2H] | 5 % | |
2 | DPC | d38 | 400 mM | |
3 | Ocellatin-LB1 | natural abundance | 1.5 mM |