Ocellatin-LB1, solution structure in SDS micelle by NMR spectroscopy
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 78.7 % (185 of 235) | 89.1 % (106 of 119) | 64.9 % (61 of 94) | 81.8 % (18 of 22) |
Backbone | 76.5 % (101 of 132) | 97.9 % (46 of 47) | 58.7 % (37 of 63) | 81.8 % (18 of 22) |
Sidechain | 84.4 % (103 of 122) | 83.3 % (60 of 72) | 86.0 % (43 of 50) | |
Aromatic | 25.0 % (1 of 4) | 50.0 % (1 of 2) | 0.0 % (0 of 2) | |
Methyl | 91.7 % (33 of 36) | 94.4 % (17 of 18) | 88.9 % (16 of 18) |
1. entity 1
GVVDILKGAA KDIAGHLASK VMXSolvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 303.15 K, pH 4, Details 2 mM Ocellatin-LB1, 1 mM DSS, 400 mM d-25 SDS, 5 % 99.75 D2O, 95% H2O/5% D2O.
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | D2O | [U-99.75 2H] | 5 % | |
2 | DSS | natural abundance | 1 mM | |
3 | Ocellatin-LB1 | natural abundance | 2 mM | |
4 | SDS | d-25 | 400 mM |