Solution NMR Structure of Unbound P18-I10
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 64.6 % (73 of 113) | 59.3 % (35 of 59) | 66.7 % (30 of 45) | 88.9 % (8 of 9) |
Backbone | 75.9 % (44 of 58) | 85.7 % (18 of 21) | 64.3 % (18 of 28) | 88.9 % (8 of 9) |
Sidechain | 58.7 % (37 of 63) | 44.7 % (17 of 38) | 80.0 % (20 of 25) | |
Aromatic | 10.0 % (1 of 10) | 20.0 % (1 of 5) | 0.0 % (0 of 5) | |
Methyl | 50.0 % (6 of 12) | 0.0 % (0 of 6) | 100.0 % (6 of 6) |
1. entity 1
RGPGRAFVTISolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 277 (±0.1) K, pH 7.2 (±0.05), Details 1.0 mM ARG-GLY-PRO-GLY-ARG-ALA-PHE-VAL-THR-ILE, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ARG-GLY-PRO-GLY-ARG-ALA-PHE-VAL-THR-ILE | natural abundance | 1.0 (±0.1) mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 277 (±0.1) K, pH 7.2 (±0.05), Details 1.00 mM [U-99% 13C; U-99% 15N] ARG-GLY-PRO-GLY-ARG-ALA-PHE-VAL-THR-ILE, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
2 | ARG-GLY-PRO-GLY-ARG-ALA-PHE-VAL-THR-ILE | [U-99% 13C; U-99% 15N] | 1.00 (±0.1) mM |