Solution structure of SH3 domain from Shank1
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 43.8 % (307 of 701) | 20.5 % (75 of 366) | 64.4 % (174 of 270) | 89.2 % (58 of 65) |
Backbone | 80.9 % (293 of 362) | 47.3 % (61 of 129) | 100.0 % (174 of 174) | 98.3 % (58 of 59) |
Sidechain | 16.9 % (66 of 391) | 5.9 % (14 of 237) | 35.1 % (52 of 148) | 0.0 % (0 of 6) |
Aromatic | 0.0 % (0 of 62) | 0.0 % (0 of 31) | 0.0 % (0 of 29) | 0.0 % (0 of 2) |
Methyl | 7.1 % (4 of 56) | 0.0 % (0 of 28) | 14.3 % (4 of 28) |
1. entity 1
MVPGRSFMAV KSYQAQAEGE ISLSKGEKIK VLSIGEGGFW EGQVKGRVGW FPSDCLEEVA NSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8 (±0.1), Details 1 mM [U-99% 13C; U-99% 15N] Shank1 SH3 domain, 20 mM Bis-Tirs, 100 mM KCl, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Shank1 SH3 domain | [U-99% 13C; U-99% 15N] | 1 mM | |
2 | Bis-Tirs | natural abundance | 20 mM | |
3 | KCl | natural abundance | 100 mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8 (±0.1), Details 1 mM [U-99% 15N] Shank1 SH3 domain, 20 mM Bis-Tris, 100 mM KCl, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
4 | Shank1 SH3 domain | [U-99% 15N] | 1 mM | |
5 | KCl | natural abundance | 100 mM | |
6 | Bis-Tris | natural abundance | 20 mM |
Solvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8 (±0.1), Details 1 mM Shank1 SH3 domain, 20 mM Bis-Tris, 100 mM KCl, 100% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | Shank1 SH3 domain | natural abundance | 1 mM | |
8 | KCl | natural abundance | 100 mM | |
9 | Bis-Tris | natural abundance | 20 mM |
Solvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8 (±0.1), Details 1 mM [U-99% 13C; U-99% 15N] Shank1 SH3 domain, 20 mM Bis-Tris, 100 mM KCl, 100% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
10 | Shank1 SH3 domain | [U-99% 13C; U-99% 15N] | 1 mM | |
11 | KCl | natural abundance | 100 mM | |
12 | Bis-Tris | natural abundance | 20 mM |