Solution structure of SH3 domain from Shank3
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 43.6 % (303 of 695) | 18.8 % (68 of 362) | 65.8 % (179 of 272) | 91.8 % (56 of 61) |
Backbone | 80.4 % (288 of 358) | 46.1 % (59 of 128) | 100.0 % (173 of 173) | 98.2 % (56 of 57) |
Sidechain | 17.0 % (66 of 388) | 3.8 % (9 of 234) | 38.0 % (57 of 150) | 0.0 % (0 of 4) |
Aromatic | 0.0 % (0 of 62) | 0.0 % (0 of 31) | 0.0 % (0 of 29) | 0.0 % (0 of 2) |
Methyl | 26.7 % (16 of 60) | 20.0 % (6 of 30) | 33.3 % (10 of 30) |
1. entity 1
MVPGRKFIAV KAHSPQGEGE IPLHRGEAVK VLSIGEGGFW EGTVKGRTGW FPADCVEEVQ MSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8, Details 1 mM [U-99% 13C; U-99% 15N] Shank3 SH3, 20 mM Bis-Tris, 100 mM KCl, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Shank3 SH3 | [U-99% 13C; U-99% 15N] | 1 mM | |
2 | Bis-Tris | natural abundance | 20 mM | |
3 | KCl | natural abundance | 100 mM |
Solvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8, Details 1 mM [U-99% 13C; U-99% 15N] Shank3 SH3, 20 mM Bis-Tris, 100 mM KCl, 100% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
4 | Shank3 SH3 | [U-99% 13C; U-99% 15N] | 1 mM | |
5 | Bis-Tris | natural abundance | 20 mM | |
6 | KCl | natural abundance | 100 mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8, Details 1 mM [U-99% 15N] Shank3 SH3, 20 mM Bis-Tris, 100 mM KCl, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | Shank3 SH3 | [U-99% 15N] | 1 mM | |
8 | Bis-Tris | natural abundance | 20 mM | |
9 | KCl | natural abundance | 100 mM |
Solvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8, Details 1 mM Shank3 SH3, 20 mM Bis-Tris, 100 mM KCl, 100% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
10 | Shank3 SH3 | natural abundance | 1 mM | |
11 | Bis-Tris | natural abundance | 20 mM | |
12 | KCl | natural abundance | 100 mM |