NMR structure of the HACS1 SH3 domain
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 71.7 % (720 of 1004) | 71.6 % (373 of 521) | 70.5 % (280 of 397) | 77.9 % (67 of 86) |
Backbone | 73.8 % (378 of 512) | 74.2 % (132 of 178) | 72.6 % (183 of 252) | 76.8 % (63 of 82) |
Sidechain | 70.4 % (401 of 570) | 70.3 % (241 of 343) | 70.0 % (156 of 223) | 100.0 % (4 of 4) |
Aromatic | 55.1 % (54 of 98) | 59.2 % (29 of 49) | 50.0 % (24 of 48) | 100.0 % (1 of 1) |
Methyl | 82.5 % (66 of 80) | 80.0 % (32 of 40) | 85.0 % (34 of 40) |
1. entity 1
GSDITSLYKK AGSSFRLDDD GPYSGPFCGR ARVHTDFTPS PYDTDSLKIK KGDIIDIICK TPMGMWTGML NNKVGNFKFI YVDVISESolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.7, Details 20 mM sodium phosphate, 150 mM sodium chloride, 0.05 % w/v sodium azide, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | entity_1 | [U-99% 13C; U-99% 15N] | 0.6 mM | |
2 | sodium phosphate | natural abundance | 20 mM | |
3 | sodium chloride | natural abundance | 150 mM | |
4 | sodium azide | natural abundance | 0.05 % w/v |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.7, Details 20 mM sodium phosphate, 150 mM sodium chloride, 0.05 % w/v sodium azide, 10 mg/mL Pf1 phage, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | entity_1 | [U-99% 13C; U-99% 15N] | 0.6 mM | |
6 | sodium phosphate | natural abundance | 20 mM | |
7 | sodium chloride | natural abundance | 150 mM | |
8 | sodium azide | natural abundance | 0.05 % w/v | |
9 | Pf1 phage | natural abundance | 10 mg/mL |