NMR solution structure of leech peptide HSTX-I
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS2:SG | 1:CYS14:SG |
2 | disulfide | sing | 1:CYS8:SG | 1:CYS19:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 77.6 % (211 of 272) | 93.5 % (130 of 139) | 58.2 % (64 of 110) | 73.9 % (17 of 23) |
Backbone | 76.5 % (104 of 136) | 95.7 % (45 of 47) | 64.2 % (43 of 67) | 72.7 % (16 of 22) |
Sidechain | 81.5 % (128 of 157) | 92.4 % (85 of 92) | 65.6 % (42 of 64) | 100.0 % (1 of 1) |
Aromatic | 37.5 % (15 of 40) | 70.0 % (14 of 20) | 0.0 % (0 of 19) | 100.0 % (1 of 1) |
Methyl | 87.5 % (21 of 24) | 100.0 % (12 of 12) | 75.0 % (9 of 12) |
1. entity 1
ACKEYWECGA FLFCIEGICV PMIXSolvent system 67% H2O/33% ACN-d3, Pressure 1 atm, Temperature 298 K, pH 4, Details 2 mg/mL HSTX-I, 67% H2O/33% ACN-d3
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | HSTX-I | natural abundance | 2 mg/mL |
Solvent system 67% D2O/33% ACN-d3, Pressure 1 atm, Temperature 298 K, pH 4, Details 2 mg/mL HSTX-I, 67% D2O/33% ACN-d3
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
2 | HSTX-I | natural abundance | 2 mg/mL |