Solution NMR structure of recifin, a cysteine-rich tyrosyl-DNA Phosphodiesterase I modulatory peptide from the marine sponge Axinella sp.
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS5:SG | 1:CYS21:SG |
2 | disulfide | sing | 1:CYS11:SG | 1:CYS39:SG |
3 | disulfide | sing | 1:CYS22:SG | 1:CYS42:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | |
---|---|---|---|
All | 78.0 % (344 of 441) | 98.0 % (248 of 253) | 51.1 % (96 of 188) |
Backbone | 78.1 % (157 of 201) | 98.8 % (80 of 81) | 64.2 % (77 of 120) |
Sidechain | 80.2 % (223 of 278) | 97.7 % (168 of 172) | 51.9 % (55 of 106) |
Aromatic | 45.8 % (38 of 83) | 90.5 % (38 of 42) | 0.0 % (0 of 41) |
Methyl | 100.0 % (14 of 14) | 100.0 % (7 of 7) | 100.0 % (7 of 7) |
1. entity 1
XEAFCYSDRF CQNYIGSIPD CCFGRGSYSF ELQPPPWECY QCSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 4.85, Details 4 mg/mL recifin, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | recifin | natural abundance | 4 mg/mL |
Solvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 4.85, Details 4 mg/mL recifin, 100% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
2 | recifin | natural abundance | 4 mg/mL |