ApoL1 N-terminal domain
GSDPESSIFI EDAIKYFKEK VSTQNLLLLL TDNEAWNGFV AAAELPRNEA DELRKALDNL ARQMIMKDKN WHDKGQQYRN WFLKEFPRLK SELEDNIRRL RALADGVQKV HKGT
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 85.7 % (1200 of 1400) | 83.9 % (616 of 734) | 88.1 % (468 of 531) | 85.9 % (116 of 135) |
Backbone | 90.9 % (616 of 678) | 89.1 % (205 of 230) | 92.0 % (310 of 337) | 91.0 % (101 of 111) |
Sidechain | 82.3 % (684 of 831) | 81.5 % (411 of 504) | 85.1 % (258 of 303) | 62.5 % (15 of 24) |
Aromatic | 85.5 % (94 of 110) | 85.5 % (47 of 55) | 84.6 % (44 of 52) | 100.0 % (3 of 3) |
Methyl | 89.8 % (106 of 118) | 89.8 % (53 of 59) | 89.8 % (53 of 59) |
1. entity 1
GSDPESSIFI EDAIKYFKEK VSTQNLLLLL TDNEAWNGFV AAAELPRNEA DELRKALDNL ARQMIMKDKN WHDKGQQYRN WFLKEFPRLK SELEDNIRRL RALADGVQKV HKGTSolvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 600 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 600 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 800 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Bruker AVANCE - 600 MHz
State isotropic, Solvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 310 K, pH 5.5, Details 0.9 mM [U-99% 13C; U-99% 15N] ApoL1 (61-172), 93% H2O/7% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ApoL1 (61-172) | [U-99% 13C; U-99% 15N] | 0.9 mM |
Properties
Disulfide bonds
NoneOther bonds (neither disulfide, covalent nor hydrogen bonds, e.g. Zinc–sulphur bond)
NoneNon-standard residues
NoneContent subtype: bmr30832_3.str
Assigned chemical shifts
--------10--------20--------30--------40--------50--------60--------70--------80--------90-------100 GSDPESSIFIEDAIKYFKEKVSTQNLLLLLTDNEAWNGFVAAAELPRNEADELRKALDNLARQMIMKDKNWHDKGQQYRNWFLKEFPRLKSELEDNIRRL |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||| ||||||| |||||||||| GSDPESSIFIEDAIKYFKEKVSTQNLLLLLTDNEAWNGFVAAAELPRNEADELRKALDNLARQMIMKDKNWHDKGQQY..WFLKEFP...SELEDNIRRL -------110---- RALADGVQKVHKGT |||||||||||||| RALADGVQKVHKGT
Comp_index_ID | Comp_ID | Atom_ID | CS value (ppm) |
---|---|---|---|
72 | HIS | HD1 | 10.453 |
111 | HIS | HD1 | 10.449 |
Atom group | # of target shifts | # of assigned shifts | Completeness (%) |
---|---|---|---|
1H chemical shifts | 734 | 614 | 83.7 |
13C chemical shifts | 531 | 466 | 87.8 |
15N chemical shifts | 135 | 114 | 84.4 |
Atom group | # of target shifts | # of assigned shifts | Completeness (%) |
---|---|---|---|
1H chemical shifts | 230 | 203 | 88.3 |
13C chemical shifts | 228 | 208 | 91.2 |
15N chemical shifts | 111 | 99 | 89.2 |
Atom group | # of target shifts | # of assigned shifts | Completeness (%) |
---|---|---|---|
1H chemical shifts | 504 | 411 | 81.5 |
13C chemical shifts | 303 | 258 | 85.1 |
15N chemical shifts | 24 | 15 | 62.5 |
Atom group | # of target shifts | # of assigned shifts | Completeness (%) |
---|---|---|---|
1H chemical shifts | 61 | 55 | 90.2 |
13C chemical shifts | 61 | 55 | 90.2 |
Atom group | # of target shifts | # of assigned shifts | Completeness (%) |
---|---|---|---|
1H chemical shifts | 55 | 47 | 85.5 |
13C chemical shifts | 52 | 44 | 84.6 |
15N chemical shifts | 3 | 3 | 100.0 |