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BMRB: 30881

Solution NMR Structure of PawL-Derived Peptide PLP-13
Authors
Payne, C.D., Rosengren, K.J.
Assembly
PLP-13
Entity
1. PLP-13 (polymer, Thiol state: not present), 8 monomers, 820.9290 Da Detail

TFGVVIAD


Formula weight
820.929 Da
Source organism
Senecio vulgaris
Exptl. method
solution NMR
Data set
assigned_chemical_shifts
Chem. Shift Complete
Sequence coverage: 100.0 %, Completeness: 71.4 %, Completeness (bb): 72.9 % Detail
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Polymer type: polypeptide(L)

Total1H13C15N
All71.4 % (60 of 84)80.0 % (32 of 40)58.3 % (21 of 36)87.5 % (7 of 8)
Backbone72.9 % (35 of 48)82.4 % (14 of 17)60.9 % (14 of 23)87.5 % (7 of 8)
Sidechain74.4 % (32 of 43)78.3 % (18 of 23)70.0 % (14 of 20)
Aromatic20.0 % (2 of 10)40.0 % (2 of 5) 0.0 % (0 of 5)
Methyl93.8 % (15 of 16)100.0 % (8 of 8)87.5 % (7 of 8)

1. entity 1

TFGVVIAD

Show sample condition
Sample

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 293 K, pH 3.5, Details 4 mg/mL PLP-13, 90% H2O/10% D2O


#NameIsotope labelingTypeConcentration
1PLP-13natural abundance4 mg/mL

Release date
2021-03-16
Citation
Structural Characterization of the PawL-Derived Peptide Family, an Ancient Subfamily of Orbitides
Payne, C.D., Fisher, M.F., Mylne, J.S., Rosengren, K.J.
J. Nat. Prod. (2021), 84, 2914-2922, PubMed 34672199 , DOI 10.1021/acs.jnatprod.1c00672 ,
Entries sharing articles BMRB: 6 entries Detail
  BMRB: 30882 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-16
  BMRB: 30883 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-22
  BMRB: 30884 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-29
  BMRB: 30885 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-38
  BMRB: 30886 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-42
  BMRB: 30887 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-46
Experiments performed 8 experiments Detail
Chemical shift validation 3 contents Detail
Keywords AEP-processed, PLANT PROTEIN, PLP, cyclic, orbitide