Solution Structure of the Zn-loaded form of a Metallothionein from Helix Pomatia
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 88.6 % (566 of 639) | 98.5 % (332 of 337) | 72.6 % (170 of 234) | 94.1 % (64 of 68) |
Backbone | 81.9 % (326 of 398) | 97.2 % (139 of 143) | 66.3 % (126 of 190) | 93.8 % (61 of 65) |
Sidechain | 99.7 % (296 of 297) | 99.5 % (193 of 194) | 100.0 % (100 of 100) | 100.0 % (3 of 3) |
Methyl | 100.0 % (16 of 16) | 100.0 % (8 of 8) | 100.0 % (8 of 8) |
1. entity 1
GSGKGKGEKC TSACRSEPCQ CGSKCQCGEG CTCAACKTCN CTSDGCKCGK ECTGPDSCKC GSSCSCKSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 (±0.2) K, pH 7 (±0.1), Details 0.5 mM, [U-13C,15N], 10 mM [U-2H] TRIS, 1 mM TSP, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | entity_1 | [U-13C; U-15N] | 0.5 mM | |
2 | TRIS | [U-2H] | 10 (±1.0) mM | |
3 | TSP | none | 1 (±0.1) mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 (±0.2) K, pH 7 (±0.1), Details 0.5 mM, [U-13C,15N], 10 mM [U-2H] TRIS, 1 mM TSP, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
4 | entity_1 | [U-13C; U-15N] | 0.5 mM | |
5 | TRIS | [U-2H] | 10 (±1.0) mM | |
6 | TSP | none | 1 (±0.1) mM |