C-SH2 domain of SHP-2 in complex with phospho-ITSM of PD-1
GPMADPTSER WFHGHLSGKE AEKLLTEKGK HGSFLVRESQ SHPGDFVLSV RTGDDKGESN DGKSKVTHVM IRCQELKYDV GGGERFDSLT DLVEHYKKNP MVETLGTVLQ LKQPLNTTR
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 94.7 % (1406 of 1485) | 98.8 % (767 of 776) | 89.8 % (518 of 577) | 91.7 % (121 of 132) |
Backbone | 93.8 % (715 of 762) | 99.2 % (263 of 265) | 90.6 % (339 of 374) | 91.9 % (113 of 123) |
Sidechain | 95.1 % (798 of 839) | 98.6 % (504 of 511) | 89.7 % (286 of 319) | 88.9 % (8 of 9) |
Aromatic | 83.3 % (85 of 102) | 92.2 % (47 of 51) | 74.0 % (37 of 50) | 100.0 % (1 of 1) |
Methyl | 95.2 % (118 of 124) | 100.0 % (62 of 62) | 90.3 % (56 of 62) |
1. entity 1
GPMADPTSER WFHGHLSGKE AEKLLTEKGK HGSFLVRESQ SHPGDFVLSV RTGDDKGESN DGKSKVTHVM IRCQELKYDV GGGERFDSLT DLVEHYKKNP MVETLGTVLQ LKQPLNTTR2. entity 2
EQTEXATIVF PSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8, Details 800 uM [U-13C; U-15N] C-SH2 domain of SHP-2, 1000 uM ITSM, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | C-SH2 domain of SHP-2 | [U-13C; U-15N] | 800 uM | |
2 | ITSM | natural abundance | 1000 uM | |
3 | NaCl | natural abundance | 150 mM | |
4 | MES (2-(N-morpholino)ethanesulfonic acid) | natural abundance | 10 mM | |
5 | TCEP (tris(2-carboxyethyl)phosphine) | natural abundance | 3 mM |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8, Details 800 uM [U-13C; U-15N] C-SH2 domain of SHP-2, 640 uM ITSM, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
6 | C-SH2 domain of SHP-2 | [U-13C; U-15N] | 800 uM | |
7 | ITSM | natural abundance | 640 uM | |
8 | NaCl | natural abundance | 150 mM | |
9 | MES (2-(N-morpholino)ethanesulfonic acid) | natural abundance | 10 mM | |
10 | TCEP (tris(2-carboxyethyl)phosphine) | natural abundance | 3 mM |