Bordetella pertussis adenylate cyclase toxin transmembrane segment 411-490 in DPC micelles
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 95.0 % (787 of 828) | 95.0 % (401 of 422) | 95.0 % (303 of 319) | 95.4 % (83 of 87) |
Backbone | 97.1 % (464 of 478) | 96.4 % (162 of 168) | 97.8 % (226 of 231) | 96.2 % (76 of 79) |
Sidechain | 93.3 % (393 of 421) | 94.1 % (239 of 254) | 92.5 % (147 of 159) | 87.5 % (7 of 8) |
Aromatic | 68.2 % (30 of 44) | 77.3 % (17 of 22) | 57.1 % (12 of 21) | 100.0 % (1 of 1) |
Methyl | 100.0 % (92 of 92) | 100.0 % (46 of 46) | 100.0 % (46 of 46) |
1. entity 1
GSRSFSLGEV SDMAAVEAAE LEMTRQVLHA GARQDDAEPG VSGASAHWGQ RALQGAQAVA AAQRLVHAIA LMTQFGRAGSSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.5, Details 450 uM [U-13C; U-15N] Cya411-490, 25 mM sodium phosphate, 100 mM sodium chloride, 1 mM TCEP, 100 mM [U-2H] DPC, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Cya411-490 | [U-13C; U-15N] | 450 uM | |
2 | sodium phosphate | natural abundance | 25 mM | |
3 | sodium chloride | natural abundance | 100 mM | |
4 | TCEP | natural abundance | 1 mM | |
5 | DPC | [U-2H] | 100 mM |