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BMRB: 34915

Single acyclic phosphonate nucleotide (R)-ZNA modification on DNA duplex

Authors

Li, X., Groaz, E., Herdewyn, P., Lescrinier, E.

Assembly

C modified (R)-ZNA

Entity

1. C modified (R)-ZNA (polymer, Thiol state: not present), 12 monomers, 3698.354 × 2 Da Detail

CGCGAATTXG CG

Total weight

7396.708 Da

Max. entity weight

3698.354 Da

Source organism

synthetic construct

Exptl. method

solution NMR

Data set

assigned_chemical_shifts, spectral_peak_list

Chemcal Shifts

¹H: 242, ¹³C: 96, ³¹P: 14 assignments Detail

ID	Entity ID	Seq ID	Comp ID	Atom ID	Atom type	Val	Ambig. code
1	1	1	DC	H1'	H	5.725
2	1	1	DC	H2'	H	2.407
3	1	1	DC	H2''	H	1.982
4	1	1	DC	H3'	H	4.696
5	1	1	DC	H4'	H	4.045
6	1	1	DC	H5	H	5.902
7	1	1	DC	H5'	H	3.694	2
8	1	1	DC	H5''	H	3.694	2
9	1	1	DC	H6	H	7.64
10	1	1	DC	H41	H	8.2
11	1	1	DC	H42	H	7.185
12	1	1	DC	C1'	C	84.958
13	1	1	DC	C2'	C	36.709
14	1	1	DC	C3'	C	75.091
15	1	1	DC	C4'	C	85.246
16	1	1	DC	C5	C	96.62
17	1	1	DC	C5'	C	60.662
18	1	2	DG	H1	H	13.085
19	1	2	DG	H1'	H	5.836
20	1	2	DG	H2'	H	2.644
21	1	2	DG	H2''	H	2.661
22	1	2	DG	H3'	H	4.944
23	1	2	DG	H4'	H	4.314
24	1	2	DG	H5'	H	4.06
25	1	2	DG	H5''	H	3.95
26	1	2	DG	H8	H	7.958
27	1	2	DG	C1'	C	81.358
28	1	2	DG	C2'	C	36.709
29	1	2	DG	C3'	C	76.731
30	1	2	DG	C4'	C	84.322
31	1	2	DG	P	P	-1.352
32	1	3	DC	H1'	H	5.568
33	1	3	DC	H2'	H	2.213
34	1	3	DC	H2''	H	1.845
35	1	3	DC	H3'	H	4.793
36	1	3	DC	H4'	H	4.134
37	1	3	DC	H5	H	5.372
38	1	3	DC	H5'	H	4.112
39	1	3	DC	H5''	H	4.053
40	1	3	DC	H6	H	7.278
41	1	3	DC	H41	H	8.287
42	1	3	DC	H42	H	6.543
43	1	3	DC	C1'	C	83.383
44	1	3	DC	C2'	C	36.268
45	1	3	DC	C3'	C	74.499
46	1	3	DC	C4'	C	82.7
47	1	3	DC	C5	C	95.656
48	1	3	DC	P	P	-1.46
49	1	4	DG	H1	H	12.8
50	1	4	DG	H1'	H	5.141
51	1	4	DG	H2'	H	2.615
52	1	4	DG	H2''	H	2.573
53	1	4	DG	H3'	H	4.928
54	1	4	DG	H4'	H	4.239
55	1	4	DG	H5'	H	4.035
56	1	4	DG	H5''	H	3.916
57	1	4	DG	H8	H	7.822
58	1	4	DG	C1'	C	80.953
59	1	4	DG	C2'	C	37.095
60	1	4	DG	C3'	C	76.22
61	1	4	DG	C4'	C	84.271
62	1	4	DG	P	P	-1.361
63	1	5	DA	H1'	H	5.925
64	1	5	DA	H2	H	7.314
65	1	5	DA	H2'	H	2.908
66	1	5	DA	H2''	H	2.777
67	1	5	DA	H3'	H	5.056
68	1	5	DA	H4'	H	4.431
69	1	5	DA	H5'	H	4.153
70	1	5	DA	H5''	H	4.083
71	1	5	DA	H8	H	8.195
72	1	5	DA	C1'	C	81.313
73	1	5	DA	C3'	C	76.455
74	1	5	DA	C4'	C	84.537
75	1	5	DA	P	P	-1.137
76	1	6	DA	H1'	H	6.145
77	1	6	DA	H2	H	7.61
78	1	6	DA	H2'	H	2.581
79	1	6	DA	H2''	H	2.878
80	1	6	DA	H3'	H	4.983
81	1	6	DA	H4'	H	4.473
82	1	6	DA	H5'	H	4.263
83	1	6	DA	H5''	H	4.217
84	1	6	DA	H8	H	8.167
85	1	6	DA	H61	H	7.251
86	1	6	DA	H62	H	6.173
87	1	6	DA	C1'	C	81.583
88	1	6	DA	C3'	C	75.681
89	1	6	DA	C4'	C	84.056
90	1	7	DT	H1'	H	5.858
91	1	7	DT	H2'	H	1.946
92	1	7	DT	H2''	H	2.481
93	1	7	DT	H3	H	13.621
94	1	7	DT	H3'	H	4.777
95	1	7	DT	H4'	H	4.178
96	1	7	DT	H5'	H	4.13
97	1	7	DT	H5''	H	4.116
98	1	7	DT	H6	H	7.125
99	1	7	DT	H71	H	1.259
100	1	7	DT	H72	H	1.259
101	1	7	DT	H73	H	1.259
102	1	7	DT	C1'	C	81.996
103	1	7	DT	C3'	C	73.802
104	1	7	DT	C4'	C	82.194
105	1	7	DT	C7	C	10.854
106	1	7	DT	P	P	-1.746
107	1	8	DT	H1'	H	5.986
108	1	8	DT	H2'	H	2.179
109	1	8	DT	H2''	H	1.999
110	1	8	DT	H3	H	14.036
111	1	8	DT	H3'	H	4.844
112	1	8	DT	H4'	H	4.176
113	1	8	DT	H5'	H	4.072
114	1	8	DT	H5''	H	3.876
115	1	8	DT	H6	H	7.426
116	1	8	DT	H71	H	1.526
117	1	8	DT	H72	H	1.526
118	1	8	DT	H73	H	1.526
119	1	8	DT	C1'	C	82.123
120	1	8	DT	C3'	C	74.553
121	1	8	DT	C4'	C	83.106
122	1	8	DT	C5'	C	61.996
123	1	8	DT	C7	C	11.15
124	1	9	CFV	CAA	C	62.941
125	1	9	CFV	CAD	C	94.956
126	1	9	CFV	HAA	H	4.1
127	1	9	CFV	HAAA	H	3.905
128	1	9	CFV	HAC	H	7.361
129	1	9	CFV	HAD	H	5.63
130	1	9	CFV	HAJ	H	4.071
131	1	9	CFV	HAL	H	3.912
132	1	9	CFV	HALA	H	3.882
133	1	9	CFV	HAQ	H	3.412
134	1	9	CFV	HAQA	H	2.944
135	1	9	CFV	HNAA	H	8.315
136	1	9	CFV	HNAF	H	6.787
137	1	9	CFV	PAM	P	14.621
138	1	10	DG	H1	H	12.922
139	1	10	DG	H1'	H	5.863
140	1	10	DG	H2'	H	2.708
141	1	10	DG	H2''	H	2.575
142	1	10	DG	H3'	H	4.957
143	1	10	DG	H4'	H	4.335
144	1	10	DG	H5'	H	4.117
145	1	10	DG	H5''	H	4.055
146	1	10	DG	H8	H	7.831
147	1	10	DG	C1'	C	81.543
148	1	10	DG	C3'	C	76.27
149	1	10	DG	C4'	C	84.258
150	1	10	DG	P	P	-0.032
151	1	11	DC	H1'	H	5.667
152	1	11	DC	H2'	H	2.315
153	1	11	DC	H2''	H	1.925
154	1	11	DC	H3'	H	4.803
155	1	11	DC	H4'	H	4.132
156	1	11	DC	H5	H	5.455
157	1	11	DC	H6	H	7.358
158	1	11	DC	H41	H	8.527
159	1	11	DC	H42	H	6.763
160	1	11	DC	C1'	C	83.226
161	1	11	DC	C2'	C	36.205
162	1	11	DC	C3'	C	73.589
163	1	11	DC	C4'	C	82.498
164	1	11	DC	C5	C	95.684
165	1	12	DG	H1	H	13.199
166	1	12	DG	H1'	H	6.146
167	1	12	DG	H2'	H	2.329
168	1	12	DG	H2''	H	2.609
169	1	12	DG	H3'	H	4.661
170	1	12	DG	H4'	H	4.159
171	1	12	DG	H5'	H	4.048
172	1	12	DG	H8	H	7.948
173	1	12	DG	C1'	C	81.646
174	1	12	DG	C2'	C	38.642
175	1	12	DG	C3'	C	70.427
176	1	12	DG	C4'	C	84.892
177	1	1	DC	H1'	H	5.725
178	1	1	DC	H2'	H	2.407
179	1	1	DC	H2''	H	1.982
180	1	1	DC	H3'	H	4.696
181	1	1	DC	H4'	H	4.045
182	1	1	DC	H5	H	5.902
183	1	1	DC	H5'	H	3.694	2
184	1	1	DC	H5''	H	3.694	2
185	1	1	DC	H6	H	7.64
186	1	1	DC	H41	H	8.2
187	1	1	DC	H42	H	7.185
188	1	1	DC	C1'	C	84.958
189	1	1	DC	C2'	C	36.709
190	1	1	DC	C3'	C	75.091
191	1	1	DC	C4'	C	85.246
192	1	1	DC	C5	C	96.62
193	1	1	DC	C5'	C	60.662
194	1	2	DG	H1	H	13.085
195	1	2	DG	H1'	H	5.836
196	1	2	DG	H2'	H	2.644
197	1	2	DG	H2''	H	2.661
198	1	2	DG	H3'	H	4.944
199	1	2	DG	H4'	H	4.314
200	1	2	DG	H5'	H	4.06
201	1	2	DG	H5''	H	3.95
202	1	2	DG	H8	H	7.958
203	1	2	DG	C1'	C	81.358
204	1	2	DG	C2'	C	36.709
205	1	2	DG	C3'	C	76.731
206	1	2	DG	C4'	C	84.322
207	1	2	DG	P	P	-1.352
208	1	3	DC	H1'	H	5.568
209	1	3	DC	H2'	H	2.213
210	1	3	DC	H2''	H	1.845
211	1	3	DC	H3'	H	4.793
212	1	3	DC	H4'	H	4.134
213	1	3	DC	H5	H	5.372
214	1	3	DC	H5'	H	4.112
215	1	3	DC	H5''	H	4.053
216	1	3	DC	H6	H	7.278
217	1	3	DC	H41	H	8.287
218	1	3	DC	H42	H	6.543
219	1	3	DC	C1'	C	83.383
220	1	3	DC	C2'	C	36.268
221	1	3	DC	C3'	C	74.499
222	1	3	DC	C4'	C	82.7
223	1	3	DC	C5	C	95.656
224	1	3	DC	P	P	-1.46
225	1	4	DG	H1	H	12.8
226	1	4	DG	H1'	H	5.141
227	1	4	DG	H2'	H	2.615
228	1	4	DG	H2''	H	2.573
229	1	4	DG	H3'	H	4.928
230	1	4	DG	H4'	H	4.239
231	1	4	DG	H5'	H	4.035
232	1	4	DG	H5''	H	3.916
233	1	4	DG	H8	H	7.822
234	1	4	DG	C1'	C	80.953
235	1	4	DG	C2'	C	37.095
236	1	4	DG	C3'	C	76.22
237	1	4	DG	C4'	C	84.271
238	1	4	DG	P	P	-1.361
239	1	5	DA	H1'	H	5.925
240	1	5	DA	H2	H	7.314
241	1	5	DA	H2'	H	2.908
242	1	5	DA	H2''	H	2.777
243	1	5	DA	H3'	H	5.056
244	1	5	DA	H4'	H	4.431
245	1	5	DA	H5'	H	4.153
246	1	5	DA	H5''	H	4.083
247	1	5	DA	H8	H	8.195
248	1	5	DA	C1'	C	81.313
249	1	5	DA	C3'	C	76.455
250	1	5	DA	C4'	C	84.537
251	1	5	DA	P	P	-1.137
252	1	6	DA	H1'	H	6.145
253	1	6	DA	H2	H	7.61
254	1	6	DA	H2'	H	2.581
255	1	6	DA	H2''	H	2.878
256	1	6	DA	H3'	H	4.983
257	1	6	DA	H4'	H	4.473
258	1	6	DA	H5'	H	4.263
259	1	6	DA	H5''	H	4.217
260	1	6	DA	H8	H	8.167
261	1	6	DA	H61	H	7.251
262	1	6	DA	H62	H	6.173
263	1	6	DA	C1'	C	81.583
264	1	6	DA	C3'	C	75.681
265	1	6	DA	C4'	C	84.056
266	1	7	DT	H1'	H	5.858
267	1	7	DT	H2'	H	1.946
268	1	7	DT	H2''	H	2.481
269	1	7	DT	H3	H	13.621
270	1	7	DT	H3'	H	4.777
271	1	7	DT	H4'	H	4.178
272	1	7	DT	H5'	H	4.13
273	1	7	DT	H5''	H	4.116
274	1	7	DT	H6	H	7.125
275	1	7	DT	H71	H	1.259
276	1	7	DT	H72	H	1.259
277	1	7	DT	H73	H	1.259
278	1	7	DT	C1'	C	81.996
279	1	7	DT	C3'	C	73.802
280	1	7	DT	C4'	C	82.194
281	1	7	DT	C7	C	10.854
282	1	7	DT	P	P	-1.746
283	1	8	DT	H1'	H	5.986
284	1	8	DT	H2'	H	2.179
285	1	8	DT	H2''	H	1.999
286	1	8	DT	H3	H	14.036
287	1	8	DT	H3'	H	4.844
288	1	8	DT	H4'	H	4.176
289	1	8	DT	H5'	H	4.072
290	1	8	DT	H5''	H	3.876
291	1	8	DT	H6	H	7.426
292	1	8	DT	H71	H	1.526
293	1	8	DT	H72	H	1.526
294	1	8	DT	H73	H	1.526
295	1	8	DT	C1'	C	82.123
296	1	8	DT	C3'	C	74.553
297	1	8	DT	C4'	C	83.106
298	1	8	DT	C5'	C	61.996
299	1	8	DT	C7	C	11.15
300	1	9	CFV	CAA	C	62.941
301	1	9	CFV	CAD	C	94.956
302	1	9	CFV	HAA	H	4.1
303	1	9	CFV	HAAA	H	3.905
304	1	9	CFV	HAC	H	7.361
305	1	9	CFV	HAD	H	5.63
306	1	9	CFV	HAJ	H	4.071
307	1	9	CFV	HAL	H	3.912
308	1	9	CFV	HALA	H	3.882
309	1	9	CFV	HAQ	H	3.412
310	1	9	CFV	HAQA	H	2.944
311	1	9	CFV	HNAA	H	8.315
312	1	9	CFV	HNAF	H	6.787
313	1	9	CFV	PAM	P	14.621
314	1	10	DG	H1	H	12.922
315	1	10	DG	H1'	H	5.863
316	1	10	DG	H2'	H	2.708
317	1	10	DG	H2''	H	2.575
318	1	10	DG	H3'	H	4.957
319	1	10	DG	H4'	H	4.335
320	1	10	DG	H5'	H	4.117
321	1	10	DG	H5''	H	4.055
322	1	10	DG	H8	H	7.831
323	1	10	DG	C1'	C	81.543
324	1	10	DG	C3'	C	76.27
325	1	10	DG	C4'	C	84.258
326	1	10	DG	P	P	-0.032
327	1	11	DC	H1'	H	5.667
328	1	11	DC	H2'	H	2.315
329	1	11	DC	H2''	H	1.925
330	1	11	DC	H3'	H	4.803
331	1	11	DC	H4'	H	4.132
332	1	11	DC	H5	H	5.455
333	1	11	DC	H6	H	7.358
334	1	11	DC	H41	H	8.527
335	1	11	DC	H42	H	6.763
336	1	11	DC	C1'	C	83.226
337	1	11	DC	C2'	C	36.205
338	1	11	DC	C3'	C	73.589
339	1	11	DC	C4'	C	82.498
340	1	11	DC	C5	C	95.684
341	1	12	DG	H1	H	13.199
342	1	12	DG	H1'	H	6.146
343	1	12	DG	H2'	H	2.329
344	1	12	DG	H2''	H	2.609
345	1	12	DG	H3'	H	4.661
346	1	12	DG	H4'	H	4.159
347	1	12	DG	H5'	H	4.048
348	1	12	DG	H8	H	7.948
349	1	12	DG	C1'	C	81.646
350	1	12	DG	C2'	C	38.642
351	1	12	DG	C3'	C	70.427
352	1	12	DG	C4'	C	84.892

Release date

2024-05-28

Citation

Impact of Single Acyclic Phosphonate Nucleotide (ZNA) Modifications on DNA Duplex Stability
Li, X., Groaz, E., Herdewijn, P., Lescrinier, E.
Chemistry (2024), 30, e202401254-e202401254, PubMed 38687344 , DOI 10.1002/chem.202401254 , Abstract

Entries sharing articles BMRB: 1 entries Detail

BMRB: 34914 released on 2024-05-28
Title Single acyclic phosphonate nucleotide (S)-ZNA modification on DNA hairpin

Experiments performed 9 experiments Detail

1 2D NOESY

Instrument

Bruker AVANCE II - 600 MHz

Sample

State isotropic, Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 100% D2O

#	Name	Isotope labeling	Type	Concentration
1	Oligo2	[U-1% 13C]		990 ug/mL

2 2D NOESY

Instrument

Bruker AVANCE II - 600 MHz

Sample

State isotropic, Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 90% H2O/10% D2O

#	Name	Isotope labeling	Type	Concentration
2	Oligo2	[U-1% 13C]		990 ug/mL

3 2D 1H-1H COSY

Instrument

Bruker AVANCE II - 600 MHz

Sample

State isotropic, Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 100% D2O

#	Name	Isotope labeling	Type	Concentration
1	Oligo2	[U-1% 13C]		990 ug/mL

4 2D 1H-13C HSQC aliphatic

Instrument

Bruker AVANCE II - 600 MHz

Sample

State isotropic, Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 100% D2O

#	Name	Isotope labeling	Type	Concentration
1	Oligo2	[U-1% 13C]		990 ug/mL

5 2D 1H-13C HSQC aromatic

Instrument

Bruker AVANCE II - 600 MHz

Sample

State isotropic, Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 100% D2O

#	Name	Isotope labeling	Type	Concentration
1	Oligo2	[U-1% 13C]		990 ug/mL

6 2D TOCSY

Instrument

Bruker AVANCE II - 600 MHz

Sample

State isotropic, Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 100% D2O

#	Name	Isotope labeling	Type	Concentration
1	Oligo2	[U-1% 13C]		990 ug/mL

7 2D 1H-31P COSY

Instrument

Bruker AVANCE - 500 MHz

Sample

State isotropic, Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 100% D2O

#	Name	Isotope labeling	Type	Concentration
1	Oligo2	[U-1% 13C]		990 ug/mL

8 2D DQF-COSY

Instrument

Bruker AVANCE II - 600 MHz

Sample

State isotropic, Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 100% D2O

#	Name	Isotope labeling	Type	Concentration
1	Oligo2	[U-1% 13C]		990 ug/mL

9 2D 1H-13C HMBC aromatic

Instrument

Bruker AVANCE II - 600 MHz

Sample

State isotropic, Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 6.38, Details 990 ug/mL [U-1% 13C] Oligo2, 100% D2O

#	Name	Isotope labeling	Type	Concentration
1	Oligo2	[U-1% 13C]		990 ug/mL

Chemical shift validation 3 contents Detail

Properties

Input source #1: Assigned chemical shifts - Assigned chemical shifts	bmr34915_3.str
Diamagnetism of the molecular assembly	True (excluding Oxygen atoms)
Whether the assembly has a disulfide bond	None
Whether the assembly has a other bond	None
Whether the assembly contains a cyclic polymer	None
Overall data processing status	Warning

Disulfide bonds

None

Other bonds (neither disulfide, covalent nor hydrogen bonds, e.g. Zinc–sulphur bond)

None

Non-standard residues

Chain_ID	Seq_ID	Comp_ID	Chem_comp_name	Experimental evidences
1	9	CFV	[(2R)-1-(4-amino-2-oxo-pyrimidin-1-yl)-3-hydroxy-propan-2-yl]oxymethylphosphonic acid	Assigned chemical shifts

Content subtype: bmr34915_3.str

#	Content subtype	Saveframe	Status	# of rows	Experiment type	Sequence coverage (%)
1	Assigned chemical shifts	assigned_chemical_shifts_1	Warning	352		100.0 (chain: 1, length: 12)
1	Chemical shift references	chem_shift_reference_1	OK	3		No information

Assigned chemical shifts

Saveframe: assigned_chemical_shifts_1

Status: Warning
Sequence coverage of experimental data
- Entity_assembly_ID: 1, Chain length: 12, Sequence coverage: 100.0%
Total number of assignments
- ¹H chemical shifts: 242
- ¹³C chemical shifts: 96
- ³¹P chemical shifts: 14

Completeness of assignments

Entity_assemble_ID: 1

Excluded Comp_ID in statistics

Comp_index_ID	Comp_ID
9	CFV

Excluded Atom_ID in statistics

Comp_index_ID	Comp_ID	Atom_ID	CS value (ppm)
1	DC	H3'	4.696
1	DC	C1'	84.958
1	DC	C2'	36.709
1	DC	C3'	75.091
1	DC	C4'	85.246
1	DC	C5	96.62
1	DC	C5'	60.662
2	DG	C1'	81.358
2	DG	C2'	36.709
2	DG	C3'	76.731
2	DG	C4'	84.322
2	DG	P	-1.352
3	DC	H3'	4.793
3	DC	C1'	83.383
3	DC	C2'	36.268
3	DC	C3'	74.499
3	DC	C4'	82.7
3	DC	C5	95.656
4	DG	C1'	80.953
4	DG	C2'	37.095
4	DG	C3'	76.22
4	DG	C4'	84.271
4	DG	P	-1.361
5	DA	C1'	81.313
5	DA	C3'	76.455
5	DA	C4'	84.537
6	DA	H61	7.251
6	DA	H62	6.173
6	DA	C1'	81.583
6	DA	C3'	75.681
6	DA	C4'	84.056
7	DT	C1'	81.996
7	DT	C3'	73.802
7	DT	C4'	82.194
7	DT	C7	10.854
7	DT	P	-1.746
8	DT	C1'	82.123
8	DT	C3'	74.553
8	DT	C4'	83.106
8	DT	C5'	61.996
8	DT	C7	11.15
10	DG	C1'	81.543
10	DG	C3'	76.27
10	DG	C4'	84.258
10	DG	P	-0.032
11	DC	H3'	4.803
11	DC	C1'	83.226
11	DC	C2'	36.205
11	DC	C3'	73.589
11	DC	C4'	82.498
11	DC	C5	95.684
12	DG	C1'	81.646
12	DG	C2'	38.642
12	DG	C3'	70.427
12	DG	C4'	84.892

All atoms

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	101	98	97.0
³¹P chemical shifts	5	2	40.0

Backbone atoms

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	71	68	95.8
³¹P chemical shifts	5	2	40.0

Side chain atoms

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	30	30	100.0

Methyl group atoms

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	2	2	100.0
¹³C chemical shifts	2	2	100.0

Aromatic group atoms

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	8	8	100.0

Histogram of normalized assigned chemical shifts

Keywords (R)-ZNA, DNA, Dickerson Drew Decamers, XNA, acyclic backbone, phosphonate linkage

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BMRB: 34915

Entries sharing articles BMRB: 1 entries Detail

Experiments performed 9 experiments Detail

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Chemical shift validation 3 contents Detail