Solution structure of arenicin-3 derivative N2
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS3:SG | 1:CYS20:SG |
2 | disulfide | sing | 1:CYS7:SG | 1:CYS16:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 85.1 % (212 of 249) | 97.7 % (126 of 129) | 65.3 % (62 of 95) | 96.0 % (24 of 25) |
Backbone | 77.0 % (97 of 126) | 92.9 % (39 of 42) | 60.3 % (38 of 63) | 95.2 % (20 of 21) |
Sidechain | 93.8 % (135 of 144) | 100.0 % (87 of 87) | 83.0 % (44 of 53) | 100.0 % (4 of 4) |
Aromatic | 100.0 % (34 of 34) | 100.0 % (17 of 17) | 100.0 % (16 of 16) | 100.0 % (1 of 1) |
Methyl | 60.0 % (12 of 20) | 100.0 % (10 of 10) | 20.0 % (2 of 10) |
1. N2
AFCWNVCVYR NAVRVCHRRC NSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 4, Details 2.0 mM NA- N2, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | N2 | natural abundance | protein | 2.0 mM |
2 | H2O | natural abundance | solvent | 90 % |
3 | D2O | [U-2H] | solvent | 10 % |