membrane-bound PD-L1-CD
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 95.1 % (371 of 390) | 94.7 % (198 of 209) | 94.4 % (135 of 143) | 100.0 % (38 of 38) |
Backbone | 96.4 % (189 of 196) | 95.6 % (65 of 68) | 95.8 % (92 of 96) | 100.0 % (32 of 32) |
Sidechain | 94.2 % (211 of 224) | 94.3 % (133 of 141) | 93.5 % (72 of 77) | 100.0 % (6 of 6) |
Aromatic | 0.0 % (0 of 4) | 0.0 % (0 of 2) | 0.0 % (0 of 2) | |
Methyl | 100.0 % (22 of 22) | 100.0 % (11 of 11) | 100.0 % (11 of 11) |
1. Programmed cell death 1 ligand 1
GPRLRKGRMM DVKKCGIQDT NSKKQSDTHL EETSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 300 K, pH 6.0, Details 0.5 mM 15N_13C_2H PD-L1-CD, 60 mM DMPG, 85 mM DHPC, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | PD-L1-CD | [U-13C; U-15N; U-2H] | protein | 0.5 mM |
2 | DHPC | natural abundance | 85 mM | |
3 | DMPG | natural abundance | 60 mM | |
4 | H2O | natural abundance | solvent | 90 % |
5 | D2O | [U-2H] | solvent | 10 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 300 K, pH 6.0, Details 0.5 mM 15N_13C PD-L1-CD, 60 mM 2H DMPG, 85 mM 2H DHPC, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
6 | PD-L1-CD | [U-13C; U-15N] | protein | 0.5 mM |
7 | DHPC | [U-2H] | 85 mM | |
8 | DMPG | [U-2H] | 60 mM | |
9 | H2O | natural abundance | solvent | 90 % |
10 | D2O | [U-2H] | solvent | 10 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 300 K, pH 6.0, Details 0.5 mM 15N_2H PD-L1-CD, 60 mM POPG, 85 mM 2H DHPC, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
11 | PD-L1-CD | [U-15N; U-2H] | protein | 0.5 mM |
12 | DHPC | [U-2H] | 85 mM | |
13 | POPG | natural abundance | 60 mM | |
14 | H2O | natural abundance | solvent | 90 % |
15 | D2O | [U-2H] | solvent | 10 % |