15N, 13C, and 1H resonance assignments of Jarastatin a disintegrin of Bothrops jararaca.
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS6:SG | 1:CYS16:SG |
2 | disulfide | sing | 1:CYS8:SG | 1:CYS21:SG |
3 | disulfide | sing | 1:CYS15:SG | 1:CYS38:SG |
4 | disulfide | sing | 1:CYS29:SG | 1:CYS35:SG |
5 | disulfide | sing | 1:CYS34:SG | 1:CYS59:SG |
6 | disulfide | sing | 1:CYS47:SG | 1:CYS66:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 94.9 % (708 of 746) | 94.8 % (368 of 388) | 96.8 % (270 of 279) | 88.6 % (70 of 79) |
Backbone | 96.7 % (414 of 428) | 96.7 % (145 of 150) | 96.7 % (203 of 210) | 97.1 % (66 of 68) |
Sidechain | 93.5 % (357 of 382) | 93.7 % (223 of 238) | 97.7 % (130 of 133) | 36.4 % (4 of 11) |
Aromatic | 100.0 % (32 of 32) | 100.0 % (16 of 16) | 100.0 % (16 of 16) | |
Methyl | 92.1 % (35 of 38) | 89.5 % (17 of 19) | 94.7 % (18 of 19) |
1. entity 1
EAGEECDCGT PGNPCCDAAT CKLRPGAQCA EGLCCDQCRF MKEGTVCRRA RGDDMDDYCN GISAGCPRNP FHASolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 293 K, pH 6
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | rJast | [U-100% 13C; U-100% 15N] | 800 uM | |
2 | sodium phosphate | natural abundance | 5 uM |