1H, 13C, and 15N resonance assignment of the vascular endothelial growth factor receptor-binding domain in complex with a receptor-blocking peptide
HHEVVKFMDV YQRSYCHPIE TLVDIFQEYP DEIEYIFKPS CVPLMRCGGC CNDEGLECVP TEESNITMQI MRIKPHQGQH IGEMSFLQHN KCECRPKKD
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 0:CYS16:SG | 1:CYS58:SG |
2 | disulfide | sing | 0:CYS47:SG | 1:CYS92:SG |
3 | disulfide | sing | 0:CYS51:SG | 1:CYS94:SG |
4 | disulfide | sing | 0:CYS41:SG | 1:CYS50:SG |
5 | disulfide | sing | 0:CYS16:SG | 1:CYS58:SG |
6 | disulfide | sing | 0:CYS47:SG | 1:CYS92:SG |
7 | disulfide | sing | 0:CYS51:SG | 1:CYS94:SG |
8 | disulfide | sing | 0:CYS41:SG | 1:CYS50:SG |
9 | disulfide | sing | 0:CYS5:SG | 2:CYS15:SG |
10 | disulfide | sing | 0:CYS5:SG | 2:CYS15:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 79.6 % (1123 of 1411) | 78.8 % (586 of 744) | 80.9 % (440 of 544) | 78.9 % (97 of 123) |
Backbone | 80.7 % (560 of 694) | 78.4 % (185 of 236) | 82.7 % (287 of 347) | 79.3 % (88 of 111) |
Sidechain | 79.3 % (657 of 828) | 79.1 % (402 of 508) | 79.9 % (246 of 308) | 75.0 % (9 of 12) |
Aromatic | 55.4 % (72 of 130) | 55.4 % (36 of 65) | 57.1 % (36 of 63) | 0.0 % (0 of 2) |
Methyl | 88.6 % (78 of 88) | 88.6 % (39 of 44) | 88.6 % (39 of 44) |
1. vascular endothelial growth factor
HHEVVKFMDV YQRSYCHPIE TLVDIFQEYP DEIEYIFKPS CVPLMRCGGC CNDEGLECVP TEESNITMQI MRIKPHQGQH IGEMSFLQHN KCECRPKKD2. v107 peptide
GGNECDIARM WEWECFERLTemperature 318 (±0.2) K, pH 7.0 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | vascular endothelial growth factor | [U-98% 13C; U-98% 15N] | 2.0 mM | |
2 | v107 peptide | 2.25 mM | ||
3 | H2O | 90 % | ||
4 | D2O | 10 % |