1H, 13C, and 15N Chemical Shift Assignments for v107 in complex with vascular endothelial growth factor
HHEVVKFMDV YQRSYCHPIE TLVDIFQEYP DEIEYIFKPS CVPLMRCGGC CNDEGLECVP TEESNITMQI MRIKPHQGQH IGEMSFLQHN KCECRPKKD
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 0:CYS16:SG | 2:CYS58:SG |
2 | disulfide | sing | 0:CYS47:SG | 2:CYS92:SG |
3 | disulfide | sing | 0:CYS51:SG | 2:CYS94:SG |
4 | disulfide | sing | 0:CYS41:SG | 2:CYS50:SG |
5 | disulfide | sing | 0:CYS16:SG | 2:CYS58:SG |
6 | disulfide | sing | 0:CYS47:SG | 2:CYS92:SG |
7 | disulfide | sing | 0:CYS51:SG | 2:CYS94:SG |
8 | disulfide | sing | 0:CYS41:SG | 2:CYS50:SG |
9 | disulfide | sing | 0:CYS5:SG | 1:CYS15:SG |
10 | disulfide | sing | 0:CYS5:SG | 1:CYS15:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 18.3 % (258 of 1411) | 18.1 % (135 of 744) | 18.6 % (101 of 544) | 17.9 % (22 of 123) |
Backbone | 18.6 % (129 of 694) | 19.1 % (45 of 236) | 18.4 % (64 of 347) | 18.0 % (20 of 111) |
Sidechain | 18.0 % (149 of 828) | 17.7 % (90 of 508) | 18.5 % (57 of 308) | 16.7 % (2 of 12) |
Aromatic | 26.2 % (34 of 130) | 26.2 % (17 of 65) | 23.8 % (15 of 63) | 100.0 % (2 of 2) |
Methyl | 22.7 % (20 of 88) | 25.0 % (11 of 44) | 20.5 % (9 of 44) |
1. v107 peptide
GGNECDIARM WEWECFERL2. vascular endothelial growth factor
HHEVVKFMDV YQRSYCHPIE TLVDIFQEYP DEIEYIFKPS CVPLMRCGGC CNDEGLECVP TEESNITMQI MRIKPHQGQH IGEMSFLQHN KCECRPKKDTemperature 308 (±0.2) K, pH 7.0 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | v107 peptide | [U-98% 13C; U-98% 15N] | 0.6 mM | |
2 | vascular endothelial growth factor | 0.9 mM |