1H Chemical Shift Assignments for TC5b
Polymer type: polypeptide(L)
Total | 1H | |
---|---|---|
All | 99.2 % (124 of 125) | 99.2 % (124 of 125) |
Backbone | 97.4 % (38 of 39) | 97.4 % (38 of 39) |
Sidechain | 100.0 % (86 of 86) | 100.0 % (86 of 86) |
Aromatic | 100.0 % (10 of 10) | 100.0 % (10 of 10) |
Methyl | 100.0 % (6 of 6) | 100.0 % (6 of 6) |
1. Trp-cage Construct 5b
NLYIQWLKDG GPSSGRPPPSTemperature 282 (±2) K, pH 7 (±0.5)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Trp-cage Construct 5b | 1.0 ~ 1.8 mM | ||
2 | phosphate buffer | 15 mM | ||
3 | H2O | 100 % |
Polymer type: polypeptide(L)
Total | 1H | |
---|---|---|
All | 99.2 % (248 of 250) | 99.2 % (248 of 250) |
Backbone | 97.4 % (76 of 78) | 97.4 % (76 of 78) |
Sidechain | 100.0 % (172 of 172) | 100.0 % (172 of 172) |
Aromatic | 100.0 % (20 of 20) | 100.0 % (20 of 20) |
Methyl | 100.0 % (12 of 12) | 100.0 % (12 of 12) |
1. Trp-cage Construct 5b
NLYIQWLKDG GPSSGRPPPSTemperature 280 (±2) K, pH 7 (±1.0)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
4 | Trp-cage Construct 5b | 1.0 ~ 1.8 mM | ||
5 | phosphate buffer | 15 mM | ||
6 | Trifluoroethanol | 30 % | ||
7 | H2O | 70 % |