Sequence-specific 1H, 13C and 15N resonance assignments of the C-terminal domain of KaiA, a circadian clock protein (reduced form)
AMARMSPADK RKLLDELRSI YRTIVLEYFN TDAKVNERID EFVSKAFFAD ISVSQVLEIH VELMDTFSKQ LKLEGRSEDI LLDYRLTLID VIAHLCEMYR RSIPREV
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 29.4 % (381 of 1297) | 15.6 % (105 of 675) | 35.5 % (182 of 513) | 86.2 % (94 of 109) |
Backbone | 58.3 % (372 of 638) | 46.5 % (99 of 213) | 55.9 % (179 of 320) | 89.5 % (94 of 105) |
Sidechain | 12.3 % (94 of 765) | 1.3 % (6 of 462) | 29.4 % (88 of 299) | 0.0 % (0 of 4) |
Aromatic | 0.0 % (0 of 90) | 0.0 % (0 of 45) | 0.0 % (0 of 45) | |
Methyl | 8.5 % (12 of 142) | 5.6 % (4 of 71) | 11.3 % (8 of 71) |
1. Thermosynechococcus KaiA
AMARMSPADK RKLLDELRSI YRTIVLEYFN TDAKVNERID EFVSKAFFAD ISVSQVLEIH VELMDTFSKQ LKLEGRSEDI LLDYRLTLID VIAHLCEMYR RSIPREVTemperature 323 (±0.5) K, pH 7.0 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Thermosynechococcus KaiA | [U-99% 13C; U-99% 15N] | 1.2 mM | |
2 | Na2HPO4 | 20.0 mM | ||
3 | NaCl | 20.0 mM |