Signal assignments and chemical-shift structural analysis of uniformly 13C, 15N-labeled peptide, mastoparan-X, by multidimensional solid-state NMR under magic-angle spinning
Polymer type: polypeptide(L)
Total | 13C | 15N | |
---|---|---|---|
All | 100.0 % (88 of 88) | 100.0 % (71 of 71) | 100.0 % (17 of 17) |
Backbone | 100.0 % (58 of 58) | 100.0 % (43 of 43) | 100.0 % (15 of 15) |
Sidechain | 100.0 % (43 of 43) | 100.0 % (41 of 41) | 100.0 % (2 of 2) |
Aromatic | 100.0 % (6 of 6) | 100.0 % (5 of 5) | 100.0 % (1 of 1) |
Methyl | 100.0 % (11 of 11) | 100.0 % (11 of 11) |
1. mastoparan-X
INWKGIAAMA KKLLGTemperature 280 (±10) K, pH 7 (±20)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | mastoparan-X | [U-95% 13C; U-95% 15N] | 100 % |