1H, 13C, and 15N Chemical Shift Assignments for DnaG-C
AAESGVSRPV PQLKRTTMRI LIGLLVQNPE LATLVPPLEN LDENKLPGLG LFRELVNTCL SQPGLTTGQL LEHYRGTNNA ATLEKLSMWD DIADKNIAEQ TFTDSLNHMF DSLLELRQEE LIARERTHGL SNEERLELWT LNQELAKK
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 57.1 % (993 of 1738) | 42.7 % (387 of 907) | 66.5 % (446 of 671) | 100.0 % (160 of 160) |
Backbone | 98.7 % (863 of 874) | 99.7 % (296 of 297) | 97.7 % (426 of 436) | 100.0 % (141 of 141) |
Sidechain | 26.4 % (265 of 1004) | 15.2 % (93 of 610) | 40.8 % (153 of 375) | 100.0 % (19 of 19) |
Aromatic | 12.2 % (9 of 74) | 18.9 % (7 of 37) | 0.0 % (0 of 35) | 100.0 % (2 of 2) |
Methyl | 18.0 % (35 of 194) | 15.5 % (15 of 97) | 20.6 % (20 of 97) |
1. DnaG-C
AAESGVSRPV PQLKRTTMRI LIGLLVQNPE LATLVPPLEN LDENKLPGLG LFRELVNTCL SQPGLTTGQL LEHYRGTNNA ATLEKLSMWD DIADKNIAEQ TFTDSLNHMF DSLLELRQEE LIARERTHGL SNEERLELWT LNQELAKKTemperature 298 (±1) K, pH 6 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | DnaG-C | [U-90% 13C; U-15N] | 0.6 mM | |
2 | phosphate buffer | 10 mM | ||
3 | DTT | 1 mM | ||
4 | NaCl | 100 mM | ||
5 | NaN3 | 0.1 % |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 66.8 % (2321 of 3476) | 64.8 % (1175 of 1814) | 62.7 % (842 of 1342) | 95.0 % (304 of 320) |
Backbone | 88.7 % (1550 of 1748) | 96.5 % (573 of 594) | 79.9 % (697 of 872) | 99.3 % (280 of 282) |
Sidechain | 50.9 % (1022 of 2008) | 49.5 % (604 of 1220) | 52.5 % (394 of 750) | 63.2 % (24 of 38) |
Aromatic | 29.7 % (44 of 148) | 55.4 % (41 of 74) | 0.0 % (0 of 70) | 75.0 % (3 of 4) |
Methyl | 53.1 % (206 of 388) | 53.6 % (104 of 194) | 52.6 % (102 of 194) |
1. DnaG-C
AAESGVSRPV PQLKRTTMRI LIGLLVQNPE LATLVPPLEN LDENKLPGLG LFRELVNTCL SQPGLTTGQL LEHYRGTNNA ATLEKLSMWD DIADKNIAEQ TFTDSLNHMF DSLLELRQEE LIARERTHGL SNEERLELWT LNQELAKKTemperature 298 (±1) K, pH 6 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
6 | DnaG-C | [U-90% 13C; U-15N] | 0.4 mM | |
7 | phosphate buffer | 10 mM | ||
8 | DTT | 1 mM | ||
9 | NaCl | 100 mM | ||
10 | NaN3 | 0.1 % |