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1H and Calpha assignments for bombinin H2
Authors
Zangger, K.
Assembly
Bombinin H2
Entity
1. Bombinin H2 (polymer, Thiol state: not present), 20 monomers, 1918.411 Da Detail

IIGPVLGLVG SALGGLLKKI


Formula weight
1918.411 Da
Source organism
Bombina variegata
Exptl. method
NMR
Refine. method
simulated annealing
Data set
assigned_chemical_shifts
Chem. Shift Complete
Sequence coverage: 100.0 %, Completeness: 44.7 %, Completeness (bb): 55.6 % Detail

Polymer type: polypeptide(L)

Total1H13C
All44.7 % (92 of 206)65.2 % (75 of 115)18.7 % (17 of 91)
Backbone55.6 % (55 of 99)86.4 % (38 of 44)30.9 % (17 of 55)
Sidechain31.1 % (38 of 122)52.1 % (37 of 71) 2.0 % (1 of 51)
Methyl21.4 % (9 of 42)42.9 % (9 of 21) 0.0 % (0 of 21)

1. Bombinin H2

IIGPVLGLVG SALGGLLKKI

Sample

Temperature 298 (±1) K, pH 5.0 (±0.2), Details Bombinin H2 in DPC micelles


#NameIsotope labelingTypeConcentration
1Bombinin H2protein3 mM
2Dodecylphosphocholine (DPC)lipid100 mM
3KPibuffer50 mM
4NaN3antimicrobial agent0.02 %

Protein Blocks Logo
Calculated from 20 models in PDB: 2AP7, Strand ID: A Detail


Release date
2007-03-26
Citation
Structures of the glycine-rich diastereomeric peptides bombinin H2 and H4
Zangger, K., Gossler, R., Khatai, L., Lohner, K., Jilek, A.
Toxicon. (2008), 52, 246-254, PubMed 18586045 , DOI 10.1016/j.toxicon.2008.05.011 ,
Related entities 1. Bombinin H2, : 1 : 3 : 19 : 1 : 31 entities Detail
Experiments performed 3 experiments Detail
nullKeywords NMR structure