Fibronecting 1F3-2F3 backbone chemical shift assignments
SGPVEVFITE TPSQPNSHPI QWNAPQPSHI SKYILRWRPK NSVGRWKEAT IPGHLNSYTI KGLKPGVVYE GQLISIQQYG HQEVTRFDFT TTSTSTPVTS NTVTGETTPF SPLVATSESV TEITASSFVV SWVSASDTVS GFRVEYELSE EGDEPQYLDL PSTATSVNIP DLLPGRKYIV NVYQISEDGE QSLILSTSQT T
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 35.2 % (805 of 2286) | 21.6 % (254 of 1175) | 41.7 % (377 of 904) | 84.1 % (174 of 207) |
Backbone | 59.4 % (697 of 1174) | 46.7 % (186 of 398) | 57.5 % (340 of 591) | 92.4 % (171 of 185) |
Sidechain | 19.1 % (249 of 1301) | 8.8 % (68 of 777) | 35.5 % (178 of 502) | 13.6 % (3 of 22) |
Aromatic | 17.0 % (32 of 188) | 18.1 % (17 of 94) | 13.3 % (12 of 90) | 75.0 % (3 of 4) |
Methyl | 16.4 % (38 of 232) | 12.1 % (14 of 116) | 20.7 % (24 of 116) |
1. 1F3-2F3
SGPVEVFITE TPSQPNSHPI QWNAPQPSHI SKYILRWRPK NSVGRWKEAT IPGHLNSYTI KGLKPGVVYE GQLISIQQYG HQEVTRFDFT TTSTSTPVTS NTVTGETTPF SPLVATSESV TEITASSFVV SWVSASDTVS GFRVEYELSE EGDEPQYLDL PSTATSVNIP DLLPGRKYIV NVYQISEDGE QSLILSTSQT TPressure 1 (±0) atm, Temperature 303 (±0.5) K, pH 7 (±0.1), Details U-15N 1F3-2F3, 150mM NaCl, 20mM NaPi, pH 7.0, 5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | 1F3-2F3 | [U-15N] | protein | 1.2 (±0.2) mM |
2 | NaCl | 150 mM | ||
3 | NaPi | 20 mM | ||
4 | D2O | 5 % | ||
5 | H2O | 95 % |
Pressure 1 (±0) atm, Temperature 303 (±0.5) K, pH 7 (±0.1), Details U-13C, 15N 1F3-2F3, 150mM NaCl, 20mM NaPi pH 7.0, 5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
6 | 1F3-2F3 | [U-13C; U-15N] | protein | |
7 | NaCl | 150 mM | ||
8 | NaPi | 20 mM | ||
9 | D2O | 5 % | ||
10 | H2O | 95 % |