1H, 13C, 15N sequence-specific backbone and sidechain resonance assignments for dockerin-containing C-terminal region of the NagH hyaluronidase from Clostridium perfringens
MDKTNLGELI NQGKSLLDES VEGFNVGEYH KGAKDGLTVE INKAEEVFNK EDATEEEINL AKESLEGAIA RFNSLLIEES TGDFNGNGKI DIGDLAMVSK NIGSTTNTSL DLNKDGSIDE YEISFINHRI LNLEHHHHHH
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 88.5 % (1397 of 1579) | 89.6 % (731 of 816) | 85.9 % (522 of 608) | 92.9 % (144 of 155) |
Backbone | 92.9 % (780 of 840) | 93.2 % (273 of 293) | 92.9 % (378 of 407) | 92.1 % (129 of 140) |
Sidechain | 85.2 % (738 of 866) | 87.6 % (458 of 523) | 80.8 % (265 of 328) | 100.0 % (15 of 15) |
Aromatic | 14.3 % (14 of 98) | 26.5 % (13 of 49) | 2.0 % (1 of 49) | |
Methyl | 97.4 % (148 of 152) | 97.4 % (74 of 76) | 97.4 % (74 of 76) |
1. fiv doc
MDKTNLGELI NQGKSLLDES VEGFNVGEYH KGAKDGLTVE INKAEEVFNK EDATEEEINL AKESLEGAIA RFNSLLIEES TGDFNGNGKI DIGDLAMVSK NIGSTTNTSL DLNKDGSIDE YEISFINHRI LNLEHHHHHHTemperature 293 (±1) K, pH 6.5 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | fiv_doc | [U-13C; U-15N] | 1 mM |