HlyII-C major cis form
DNQKALEEQM NSINSVNDKL NKGKGKLSLS MNGNQLKATS SNAGYGISYE DKNWGIFVNG EKVYTFNEKS TVGNISNDIN KLNIKGPYIE IKQI
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 94.0 % (1043 of 1109) | 95.7 % (559 of 584) | 90.0 % (371 of 412) | 100.0 % (113 of 113) |
Backbone | 99.3 % (558 of 562) | 99.0 % (194 of 196) | 99.3 % (271 of 273) | 100.0 % (93 of 93) |
Sidechain | 90.0 % (569 of 632) | 94.1 % (365 of 388) | 82.1 % (184 of 224) | 100.0 % (20 of 20) |
Aromatic | 51.6 % (33 of 64) | 100.0 % (32 of 32) | 0.0 % (0 of 31) | 100.0 % (1 of 1) |
Methyl | 95.5 % (84 of 88) | 95.5 % (42 of 44) | 95.5 % (42 of 44) |
1. HlyIIC-cis (major)
DNQKALEEQM NSINSVNDKL NKGKGKLSLS MNGNQLKATS SNAGYGISYE DKNWGIFVNG EKVYTFNEKS TVGNISNDIN KLNIKGPYIE IKQISolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 273 K, pH 6.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | HlyIIC-cis | [U-99% 13C; U-99% 15N] | 1.0 mM | |
2 | sodium phosphate | natural abundance | 20 mM | |
3 | EDTA | natural abundance | 1 mM | |
4 | AEBSF | natural abundance | 1 mM | |
5 | sodium azide | natural abundance | 0.05 % w/v |
Solvent system 100% D2O, Pressure 1 atm, Temperature 273 K, pH 6.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
6 | HlyIIC-cis | [U-99% 15N] | 1.0 mM | |
7 | sodium phosphate | natural abundance | 20 mM | |
8 | EDTA | natural abundance | 1 mM | |
9 | AEBSF | natural abundance | 1 mM | |
10 | sodium azide | natural abundance | 0.05 % w/v |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 273 K, pH 6.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
11 | HlyIIC-cis | [U-99% 15N] | 1.0 mM | |
12 | sodium phosphate | natural abundance | 20 mM | |
13 | EDTA | natural abundance | 1 mM | |
14 | AEBSF | natural abundance | 1 mM | |
15 | sodium azide | natural abundance | 0.05 % w/v |
Solvent system 100% D2O, Pressure 1 atm, Temperature 273 K, pH 6.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
16 | HlyIIC-cis | [U-99% 13C; U-99% 15N] | 1.0 mM | |
17 | sodium phosphate | natural abundance | 20 mM | |
18 | EDTA | natural abundance | 1 mM | |
19 | AEBSF | natural abundance | 1 mM | |
20 | sodium azide | natural abundance | 0.05 % w/v |