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Found 1 Document (0.421 seconds)

BMRB: 30887

Solution NMR Structure of PawL-Derived Peptide PLP-46

Authors

Payne, C.D., Rosengren, K.J.

Assembly

PLP-46

Entity

1. PLP-46 (polymer, Thiol state: not present), 7 monomers, 777.8623 Da Detail

GYITPLD

Formula weight

777.8623 Da

Source organism

Parthenium argentatum

Exptl. method

solution NMR

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 83.5 %, Completeness (bb): 77.5 % Detail

Polymer type: polypeptide(L)

	Total	¹H	¹³C	¹⁵N
All	83.5 % (66 of 79)	97.5 % (39 of 40)	66.7 % (22 of 33)	83.3 % (5 of 6)
Backbone	77.5 % (31 of 40)	92.9 % (13 of 14)	65.0 % (13 of 20)	83.3 % (5 of 6)
Sidechain	91.1 % (41 of 45)	100.0 % (26 of 26)	78.9 % (15 of 19)
Aromatic	50.0 % (4 of 8)	100.0 % (4 of 4)	0.0 % (0 of 4)
Methyl	100.0 % (10 of 10)	100.0 % (5 of 5)	100.0 % (5 of 5)

1. entity 1

GYITPLD

Show sample condition

Sample

Solvent system 99.5% CD3CN, Pressure 1 atm, Temperature 298 K, pH 3.5, Details 2 mg/mL PLP-46, 99.5% CD3CN

#	Name	Isotope labeling	Type	Concentration
1	PLP-46	natural abundance		2 mg/mL

Release date

2021-03-16

Citation

Structural Characterization of the PawL-Derived Peptide Family, an Ancient Subfamily of Orbitides
Payne, C.D., Fisher, M.F., Mylne, J.S., Rosengren, K.J.
J. Nat. Prod. (2021), 84, 2914-2922, PubMed 34672199 , DOI 10.1021/acs.jnatprod.1c00672 , Abstract

Entries sharing articles BMRB: 6 entries Detail

  BMRB: 30881 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-13
  BMRB: 30882 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-16
  BMRB: 30883 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-22
  BMRB: 30884 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-29
  BMRB: 30885 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-38
  BMRB: 30886 released on 2021-03-16
    Title Solution NMR Structure of PawL-Derived Peptide PLP-42

Experiments performed 8 experiments Detail

Chemical shift validation 3 contents Detail

#	Content subtype	Saveframe	Status	# of rows	Experiment type	Sequence coverage (%)
1	Assigned chemical shifts	assigned_chemical_shifts_1	OK	76		100.0 (chain: 1, length: 7)
1	Chemical shift references	chem_shift_reference_1	OK	3		No information

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	40	39	97.5
¹³C chemical shifts	33	22	66.7
¹⁵N chemical shifts	6	5	83.3

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	14	13	92.9
¹³C chemical shifts	14	7	50.0
¹⁵N chemical shifts	6	5	83.3

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	26	26	100.0
¹³C chemical shifts	19	15	78.9

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	5	5	100.0
¹³C chemical shifts	5	5	100.0

Atom group	# of target shifts	# of assigned shifts	Completeness (%)
¹H chemical shifts	4	4	100.0
¹³C chemical shifts	4	0	0.0

Keywords AEP-processed, Cyclic, Orbitide, PLANT PROTEIN, PLP

Input source #1: Assigned chemical shifts - Assigned chemical shifts	bmr30887_3.str
Diamagnetism of the molecular assembly	True (excluding Oxygen atoms)
Whether the assembly has a disulfide bond	None
Whether the assembly has a other bond	None
Whether the assembly contains a cyclic polymer	None
Overall data processing status	OK

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Found 1 Document (0.421 seconds)

BMRB: 30887

Sample

Entries sharing articles BMRB: 6 entries Detail

Experiments performed 8 experiments Detail

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Chemical shift validation 3 contents Detail