NMR Structure of Ac-hGal(17-30)NH2, an N-terminally acetylated fragment of the C-terminus of human galanin
Polymer type: polypeptide(L)
Total | 1H | |
---|---|---|
All | 93.7 % (74 of 79) | 93.7 % (74 of 79) |
Backbone | 93.3 % (28 of 30) | 93.3 % (28 of 30) |
Sidechain | 93.9 % (46 of 49) | 93.9 % (46 of 49) |
Aromatic | 71.4 % (5 of 7) | 71.4 % (5 of 7) |
Methyl | 100.0 % (3 of 3) | 100.0 % (3 of 3) |
1. entity 1
XGNHRSFSDK NGLTSXSolvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 298 K, pH 4.6 (±0.02), Details 2 mM Ac-hGal(17-30)-NH2, 4.14 mM [U-2H] sodium acetate, 5.86 mM [U-2H] acetic acid, 95% H2O/5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Ac-hGal(17-30)-NH2 | natural abundance | 2 mM | |
2 | sodium acetate | [U-2H] | 4.14 mM | |
3 | acetic acid | [U-2H] | 5.86 mM |