De-ubiquitinating function of ataxin-3: insights from the solution structure of the Josephin domain
MPLGSMESIF HEKQEGSLCA QHCLNNLLQG EYFSPVELSS IAHQLDEEER MRMAEGGVTS EDYRTFLQQP SGNMDDSGFF SIQVISNALK VWGLELILFN SPEYQRLRID PINERSFICN YKEHWFTVRK LGKQWFNLNS LLTGPELISD TYLALFLAQL QQEGYSIFVV KGDLPDCEAD QLLQMIRVQQ
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 89.9 % (2055 of 2286) | 91.9 % (1096 of 1193) | 86.3 % (761 of 882) | 93.8 % (198 of 211) |
Backbone | 95.6 % (1076 of 1126) | 96.6 % (372 of 385) | 94.6 % (528 of 558) | 96.2 % (176 of 183) |
Sidechain | 84.5 % (1131 of 1338) | 89.0 % (719 of 808) | 77.9 % (391 of 502) | 75.0 % (21 of 28) |
Aromatic | 61.0 % (128 of 210) | 81.0 % (85 of 105) | 39.2 % (40 of 102) | 100.0 % (3 of 3) |
Methyl | 95.0 % (190 of 200) | 96.0 % (96 of 100) | 94.0 % (94 of 100) |
1. ataxin-3 josephin domain
MPLGSMESIF HEKQEGSLCA QHCLNNLLQG EYFSPVELSS IAHQLDEEER MRMAEGGVTS EDYRTFLQQP SGNMDDSGFF SIQVISNALK VWGLELILFN SPEYQRLRID PINERSFICN YKEHWFTVRK LGKQWFNLNS LLTGPELISD TYLALFLAQL QQEGYSIFVV KGDLPDCEAD QLLQMIRVQQTemperature 298 (±2) K, pH 6.4 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ataxin-3 josephin domain | [U-100% 13C; U-100% 15N] | 1.5 mM | |
2 | potassium phospate buffer | 20 mM |