Backbone 1H, 13C, and 15N Chemical Shift Assignments for the first dsRBD of protein HYL1
GHMMTSTDVS SGVSNCYVFK SRLQEYAQKY KLPTPVYEIV KEGPSHKSLF QSTVILDGVR YNSLPGFFNR KAAEQSAAEV ALRELAKSSE LSQCVSQPVH ETG
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 45.5 % (538 of 1182) | 29.5 % (181 of 614) | 59.7 % (275 of 461) | 76.6 % (82 of 107) |
Backbone | 83.1 % (505 of 608) | 76.3 % (158 of 207) | 87.8 % (266 of 303) | 82.7 % (81 of 98) |
Sidechain | 17.6 % (118 of 671) | 5.7 % (23 of 407) | 36.9 % (94 of 255) | 11.1 % (1 of 9) |
Aromatic | 0.0 % (0 of 92) | 0.0 % (0 of 46) | 0.0 % (0 of 46) | |
Methyl | 17.3 % (18 of 104) | 11.5 % (6 of 52) | 23.1 % (12 of 52) |
1. HYL1 dsRBD 1
GHMMTSTDVS SGVSNCYVFK SRLQEYAQKY KLPTPVYEIV KEGPSHKSLF QSTVILDGVR YNSLPGFFNR KAAEQSAAEV ALRELAKSSE LSQCVSQPVH ETGSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | HYL1 dsRBD 1 | [U-100% 13C; U-100% 15N] | 0.5 mM | |
2 | sodium phosphate | natural abundance | 100 mM | |
3 | sodium chloride | natural abundance | 50 mM | |
4 | DTT | natural abundance | 10 mM | |
5 | sodium azide | natural abundance | 0.05 % | |
6 | H2O | natural abundance | 90 % | |
7 | D2O | natural abundance | 10 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
8 | HYL1 dsRBD 1 | [U-100% 13C; U-100% 15N] | 0.5 mM | |
9 | sodium phosphate | natural abundance | 100 mM | |
10 | sodium chloride | natural abundance | 50 mM | |
11 | DTT | natural abundance | 10 mM | |
12 | sodium azide | natural abundance | 0.05 % | |
13 | C12E5 | natural abundance | 5 % | |
14 | Hexanol | natural abundance | 0.2 % | |
15 | H2O | natural abundance | 90 % | |
16 | D2O | natural abundance | 10 % |