Ocellatin-F1, solution structure in SDS micelle by NMR spectroscopy
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 82.3 % (228 of 277) | 89.4 % (127 of 142) | 70.6 % (77 of 109) | 92.3 % (24 of 26) |
Backbone | 80.0 % (120 of 150) | 100.0 % (53 of 53) | 61.1 % (44 of 72) | 92.0 % (23 of 25) |
Sidechain | 87.2 % (130 of 149) | 83.1 % (74 of 89) | 93.2 % (55 of 59) | 100.0 % (1 of 1) |
Aromatic | 25.0 % (1 of 4) | 50.0 % (1 of 2) | 0.0 % (0 of 2) | |
Methyl | 100.0 % (40 of 40) | 100.0 % (20 of 20) | 100.0 % (20 of 20) |
1. entity 1
GVVDILKGAA KDIAGHLASK VMNKLXSolvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 323.15 K, pH 4, Details 2 mM Ocellatin-F1, 1 mM DSS, 5 % 99.75 D2O, 400 mM d-25 SDS, 95% H2O/5% D2O.
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | D2O | [U-99.75 2H] | 5 % | |
2 | DSS | natural abundance | 1 mM | |
3 | Ocellatin-F1 | natural abundance | 2 mM | |
4 | SDS | d-25 | 400 mM |