Fibronectin 2F3 chemical shift assignments
GPLGSHLVAT SESVTEITAS SFVVSWVSAS DTVSGFRVEY ELSEEGDEPQ YLDLPSTATS VNIPDLLPGR KYIVNVYQIS EDGEQSLILS TSQTT
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 90.6 % (938 of 1035) | 98.3 % (516 of 525) | 79.2 % (327 of 413) | 97.9 % (95 of 97) |
Backbone | 83.6 % (468 of 560) | 97.9 % (187 of 191) | 69.2 % (193 of 279) | 97.8 % (88 of 90) |
Sidechain | 99.1 % (559 of 564) | 98.5 % (329 of 334) | 100.0 % (223 of 223) | 100.0 % (7 of 7) |
Aromatic | 100.0 % (68 of 68) | 100.0 % (34 of 34) | 100.0 % (33 of 33) | 100.0 % (1 of 1) |
Methyl | 100.0 % (122 of 122) | 100.0 % (61 of 61) | 100.0 % (61 of 61) |
1. 2F3
GPLGSHLVAT SESVTEITAS SFVVSWVSAS DTVSGFRVEY ELSEEGDEPQ YLDLPSTATS VNIPDLLPGR KYIVNVYQIS EDGEQSLILS TSQTTPressure 1 (±0) atm, Temperature 303 (±0.5) K, pH 7.0 (±0.1), Details U-15N 2F3, 20mM NaCl, 20mM NaPi, pH 7.0, 5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | 2F3 | [U-15N] | protein | 2 (±0.2) mM |
2 | NaCl | 20 mM | ||
3 | NaPi | 20 mM | ||
4 | D2O | 5 % | ||
5 | H2O | 95 % |
Pressure 1 (±0) atm, Temperature 303 (±0.5) K, pH 7.0 (±0.1), Details U-13C,15N 2F3, 20mM NaCl, 20mM NaPi pH 7.0, 5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
6 | 2F3 | [U-13C; U-15N] | protein | 1.5 (±0.1) mM |
7 | NaCl | 20 mM | ||
8 | NaPi | 20 mM | ||
9 | D2O | 5 % | ||
10 | H2O | 95 % |