Backbone 1H, 13C, and 15N Chemical Shift Assignments for dSUMO
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 87.2 % (908 of 1041) | 84.9 % (465 of 548) | 90.4 % (356 of 394) | 87.9 % (87 of 99) |
Backbone | 97.9 % (523 of 534) | 96.2 % (179 of 186) | 98.5 % (257 of 261) | 100.0 % (87 of 87) |
Sidechain | 79.3 % (466 of 588) | 79.0 % (286 of 362) | 84.1 % (180 of 214) | 0.0 % (0 of 12) |
Aromatic | 29.6 % (16 of 54) | 59.3 % (16 of 27) | 0.0 % (0 of 27) | |
Methyl | 97.6 % (80 of 82) | 100.0 % (41 of 41) | 95.1 % (39 of 41) |
1. dSUMO
GSMSDEKKGG ETEHINLKVL GQDNAVVQFK IKKHTPLRKL MNAYCDRAGL SMQVVRFRFD GQPINENDTP TSLEMEEGDT IEVYQQQTGGTemperature 300 K, pH 5.6 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | dSUMO | [U-13C; U-15N] | protein | 1 (±0.1) mM |
2 | Sodium Phosphate | buffer | 100 mM |