Backbone and Side Chain 1H, 13C and 15N Chemical Shift Assignments for Sporulation Phosphotransferase F Mutant H101A
MMNEKILIVD DQYGIRILLN EVFNKEGYQT FQAANGLQAL DIVTKERPDL VLLDMKIPGM DGIEILKRMK VIDENIRVII MTAYGELDMI QESKELGALT AFAKPFDIDE IRDAVKKYLP LKSNLEHHHH HH
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 81.8 % (1309 of 1601) | 78.1 % (653 of 836) | 84.2 % (527 of 626) | 92.8 % (129 of 139) |
Backbone | 94.8 % (743 of 784) | 94.8 % (253 of 267) | 95.1 % (370 of 389) | 93.8 % (120 of 128) |
Sidechain | 73.0 % (688 of 942) | 70.5 % (401 of 569) | 76.8 % (278 of 362) | 81.8 % (9 of 11) |
Aromatic | 10.4 % (10 of 96) | 18.8 % (9 of 48) | 2.1 % (1 of 48) | |
Methyl | 87.8 % (151 of 172) | 86.0 % (74 of 86) | 89.5 % (77 of 86) |
1. Spo0FH101A
MMNEKILIVD DQYGIRILLN EVFNKEGYQT FQAANGLQAL DIVTKERPDL VLLDMKIPGM DGIEILKRMK VIDENIRVII MTAYGELDMI QESKELGALT AFAKPFDIDE IRDAVKKYLP LKSNLEHHHH HHPressure 1 atm, Temperature 298 K, pH 6.9
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Spo0FH101A | [U-99% 13C; U-99% 15N] | 1.0 ~ 2.0 mM | |
2 | TRIS | none | 25 mM | |
3 | potassium chloride | none | 50 mM |