NMR assignment and structure of a peptide derived from the fusion peptide of HIV-1 gp41 in the presence of dodecylphosphocholine micelles
Polymer type: polypeptide(L)
Total | 1H | |
---|---|---|
All | 94.8 % (200 of 211) | 94.8 % (200 of 211) |
Backbone | 94.5 % (69 of 73) | 94.5 % (69 of 73) |
Sidechain | 94.9 % (131 of 138) | 94.9 % (131 of 138) |
Aromatic | 81.8 % (18 of 22) | 81.8 % (18 of 22) |
Methyl | 100.0 % (20 of 20) | 100.0 % (20 of 20) |
1. entity 1
GIGAFGLLGF LAAGSKKXKN EQELLELDKW ASLWNSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8, Details 0.6 mM scrFP-tag, 20 mM [U-98% 2H] DPC, 2.0 mM HEPES, 90 % H2O, 10 % [U-99% 2H] D2O, 0.1 mM DSS, 90% H2O/10% D2O.
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | D2O | [U-99% 2H] | 10 % | |
2 | DPC | [U-98% 2H] | 20 mM | |
3 | DSS | natural abundance | 0.1 mM | |
4 | H2O | natural abundance | 90 % | |
5 | HEPES | natural abundance | 2.0 mM | |
6 | scrFP-tag | natural abundance | 0.6 (±0.1) mM |